{(R)-1-[(S)-1-((1S,2S)-1-Hydrazinocarbonyl-2-methyl-butylcarbamoyl)-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-2-methylsulfanyl-ethyl}-carbamic acid tert-butyl ester

Base Information

• Chemical Name: {(R)-1-[(S)-1-((1S,2S)-1-Hydrazinocarbonyl-2-methyl-butylcarbamoyl)-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-2-methylsulfanyl-ethyl}-carbamic acid tert-butyl ester
• CAS No.: 127565-26-8
• Molecular Formula: C₂₄H₃₉N₅O₆S
• Molecular Weight: 525.67

Synonyms:

Chemical Property of {(R)-1-[(S)-1-((1S,2S)-1-Hydrazinocarbonyl-2-methyl-butylcarbamoyl)-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-2-methylsulfanyl-ethyl}-carbamic acid tert-butyl ester

Chemical Property:

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Technology Process of {(R)-1-[(S)-1-((1S,2S)-1-Hydrazinocarbonyl-2-methyl-butylcarbamoyl)-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-2-methylsulfanyl-ethyl}-carbamic acid tert-butyl ester

There total 3 articles about {(R)-1-[(S)-1-((1S,2S)-1-Hydrazinocarbonyl-2-methyl-butylcarbamoyl)-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-2-methylsulfanyl-ethyl}-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(2S,3S)-2-[(S)-2-((R)-2-tert-Butoxycarbonylamino-3-methylsulfanyl-propionylamino)-3-(4-hydroxy-phenyl)-propionylamino]-3-methyl-pentanoic acid methyl ester (127565-19-9) → {(R)-1-[(S)-1-((1S,2S)-1-Hydrazinocarbonyl-2-methyl-butylcarbamoyl)-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-2-methylsulfanyl-ethyl}-carbamic acid tert-butyl ester (127565-26-8)

Guidance literature:

With hydrazine;

DOI:10.1007/BF00598080

Reference yield:

N-(tert-butoxycarbonyl)-S-methyl-L-cysteine (16947-80-1) → {(R)-1-[(S)-1-((1S,2S)-1-Hydrazinocarbonyl-2-methyl-butylcarbamoyl)-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-2-methylsulfanyl-ethyl}-carbamic acid tert-butyl ester (127565-26-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / DCHC / dimethylformamide / 1) -5 deg C, 24h, 2) RT, 3h

2: 92 percent / N₂H₄

With hydrazine; In N,N-dimethyl-formamide;

DOI:10.1007/BF00598080

Reference yield:

HTyr-IleOMe (101399-36-4) → {(R)-1-[(S)-1-((1S,2S)-1-Hydrazinocarbonyl-2-methyl-butylcarbamoyl)-2-(4-hydroxy-phenyl)-ethylcarbamoyl]-2-methylsulfanyl-ethyl}-carbamic acid tert-butyl ester (127565-26-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / DCHC / dimethylformamide / 1) -5 deg C, 24h, 2) RT, 3h

2: 92 percent / N₂H₄

With hydrazine; In N,N-dimethyl-formamide;

DOI:10.1007/BF00598080

upstream raw materials:

(2S,3S)-2-[(S)-2-((R)-2-tert-Butoxycarbonylamino-3-methylsulfanyl-propionylamino)-3-(4-hydroxy-phenyl)-propionylamino]-3-methyl-pentanoic acid methyl ester

N-(tert-butoxycarbonyl)-S-methyl-L-cysteine

HTyr-IleOMe

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