[(4S,5R)-5-((E)-Pentadec-1-enyl)-2-phenyl-4,5-dihydro-oxazol-4-yl]-methanol

Base Information Edit

Chemical Name:[(4S,5R)-5-((E)-Pentadec-1-enyl)-2-phenyl-4,5-dihydro-oxazol-4-yl]-methanol
CAS No.:102874-34-0
Molecular Formula:C₂₅H₃₉NO₂
Molecular Weight:385.59
Hs Code.:
Mol file:102874-34-0.mol

Synonyms:

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Chemical Property of [(4S,5R)-5-((E)-Pentadec-1-enyl)-2-phenyl-4,5-dihydro-oxazol-4-yl]-methanol Edit

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Technology Process of [(4S,5R)-5-((E)-Pentadec-1-enyl)-2-phenyl-4,5-dihydro-oxazol-4-yl]-methanol

There total 7 articles about [(4S,5R)-5-((E)-Pentadec-1-enyl)-2-phenyl-4,5-dihydro-oxazol-4-yl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6847-14-9,14086-91-0,19949-63-4,61949-16-4
N-benzoyl-D-glucosamine

: 102874-34-0,144150-69-6,144150-70-9
[(4S,5R)-5-((E)-Pentadec-1-enyl)-2-phenyl-4,5-dihydro-oxazol-4-yl]-methanol

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / conc. H₂SO₄ / 12 h / Ambient temperature

2: 41 percent / trifluoromethanesulfonic anhydride, pyridine / CH₂Cl₂ / a) 0 deg C, 1 h, b) room temperature, 3 h

3: 92 percent / NaBH₄ / methanol / 1 h / 0 °C

4: BF₃*OEt₂, PhSH / CH₂Cl₂ / 10 h / 0 °C

5: NaIO₄, NaHCO₃ / methanol; H₂O / 24 h / 0 deg C to room temperature; pH: 7.5-8.0

6: 1) BuLi / 1) THF, toluene, -30 to 0 deg C, 2) to room temperature, 3 h

With pyridine; sodium tetrahydroborate; sodium periodate; n-butyllithium; sulfuric acid; boron trifluoride diethyl etherate; sodium hydrogencarbonate; thiophenol; trifluoromethanesulfonic acid anhydride; In methanol; dichloromethane; water;

Reference yield:

: (1R,2R)-1-((4S,5S)-4-Hydroxymethyl-2-phenyl-4,5-dihydro-oxazol-5-yl)-propane-1,2,3-triol

: 102874-34-0,144150-69-6,144150-70-9
[(4S,5R)-5-((E)-Pentadec-1-enyl)-2-phenyl-4,5-dihydro-oxazol-4-yl]-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: NaIO₄, NaHCO₃ / methanol; H₂O / 24 h / 0 deg C to room temperature; pH: 7.5-8.0

2: 1) BuLi / 1) THF, toluene, -30 to 0 deg C, 2) to room temperature, 3 h

With sodium periodate; n-butyllithium; sodium hydrogencarbonate; In methanol; water;

Reference yield:

: N-Benzoyl-4,6-O-ethylidene-D-glucosamine

: 102874-34-0,144150-69-6,144150-70-9
[(4S,5R)-5-((E)-Pentadec-1-enyl)-2-phenyl-4,5-dihydro-oxazol-4-yl]-methanol

Guidance literature:: Multi-step reaction with 5 steps

1: 41 percent / trifluoromethanesulfonic anhydride, pyridine / CH₂Cl₂ / a) 0 deg C, 1 h, b) room temperature, 3 h

2: 92 percent / NaBH₄ / methanol / 1 h / 0 °C

3: BF₃*OEt₂, PhSH / CH₂Cl₂ / 10 h / 0 °C

4: NaIO₄, NaHCO₃ / methanol; H₂O / 24 h / 0 deg C to room temperature; pH: 7.5-8.0

5: 1) BuLi / 1) THF, toluene, -30 to 0 deg C, 2) to room temperature, 3 h

With pyridine; sodium tetrahydroborate; sodium periodate; n-butyllithium; boron trifluoride diethyl etherate; sodium hydrogencarbonate; thiophenol; trifluoromethanesulfonic acid anhydride; In methanol; dichloromethane; water;