1-(o-chlorophenyl)-2-bromo-2-chloro-1-propyl trifluoroacetate

Base Information

Chemical Name:1-(o-chlorophenyl)-2-bromo-2-chloro-1-propyl trifluoroacetate
CAS No.:344336-96-5
Molecular Formula:C₁₁H₈BrCl₂F₃O₂
Molecular Weight:379.989
Hs Code.:

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Chemical Property of 1-(o-chlorophenyl)-2-bromo-2-chloro-1-propyl trifluoroacetate

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Technology Process of 1-(o-chlorophenyl)-2-bromo-2-chloro-1-propyl trifluoroacetate

There total 4 articles about 1-(o-chlorophenyl)-2-bromo-2-chloro-1-propyl trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 81671-54-7
1-(o-chlorophenyl)-2-bromo-2-chloro-1-propanol

: 407-25-0
trifluoroacetic anhydride

: 344336-96-5
1-(o-chlorophenyl)-2-bromo-2-chloro-1-propyl trifluoroacetate

Guidance literature:: In diethyl ether; for 18h; Ambient temperature;
DOI:10.1021/jo00135a027

Reference yield:

: 6323-18-8
2-chloropropiophenone

: 344336-96-5
1-(o-chlorophenyl)-2-bromo-2-chloro-1-propyl trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Cl₂, 2.) HCl(gas) / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) RT, overnight

2: 84 percent / N-bromosuccinimide / CCl₄ / 6 h / Heating; Irradiation

3: 90 percent / diisobutylaluminum hydride / hexane / 2 h / Ambient temperature

4: 99 percent / diethyl ether / 18 h / Ambient temperature

With hydrogenchloride; N-Bromosuccinimide; chlorine; diisobutylaluminium hydride; In tetrachloromethane; diethyl ether; hexane;
DOI:10.1021/jo00135a027

Reference yield:

: 81671-55-8
1-(o-chlorophenyl)-2-chloro-1-propanone

: 344336-96-5
1-(o-chlorophenyl)-2-bromo-2-chloro-1-propyl trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / N-bromosuccinimide / CCl₄ / 6 h / Heating; Irradiation

2: 90 percent / diisobutylaluminum hydride / hexane / 2 h / Ambient temperature

3: 99 percent / diethyl ether / 18 h / Ambient temperature

With N-Bromosuccinimide; diisobutylaluminium hydride; In tetrachloromethane; diethyl ether; hexane;
DOI:10.1021/jo00135a027