(1-diphenylphosphino-2-diphenylarsinoethane)chromium tetracarbonyl

Base Information

Chemical Name:(1-diphenylphosphino-2-diphenylarsinoethane)chromium tetracarbonyl
CAS No.:40545-10-6
Molecular Formula:C₃₀H₂₄AsCrO₄P
Molecular Weight:606.41
Hs Code.:

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Chemical Property of (1-diphenylphosphino-2-diphenylarsinoethane)chromium tetracarbonyl

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Technology Process of (1-diphenylphosphino-2-diphenylarsinoethane)chromium tetracarbonyl

There total 1 articles about (1-diphenylphosphino-2-diphenylarsinoethane)chromium tetracarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 58751-37-4
pentacarbonyl(dimethyloxosulfonium methylide)chromium⁽⁰⁾

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: 40545-10-6
(1-diphenylphosphino-2-diphenylarsinoethane)chromium tetracarbonyl

: 95531-66-1
tetracarbonyl[(2-(diphenylarsino)ethyl)diphenylphosphonium methylide-α-C,ω-As]chromium(0)

Guidance literature:: In toluene; under inert atmosphere; a mixture of Cr-complex and P-compound in toluene stirred at 60°C for 7 h; stirred at 20°C for 16 h; filtered; evapd.; recrystd. from CH2Cl2/hexane at 0°C; hexane added; elem. anal.;

Reference yield:

: 40545-10-6
(1-diphenylphosphino-2-diphenylarsinoethane)chromium tetracarbonyl

: 60019-72-9
dibromo(1-diphenylphosphino-2-diphenylarsinoethane)chromium dicarbonyl

Guidance literature:: With bromine; In hexane; benzene; N2-atmosphere; dropwise addn. of bromine (in hexane) to Cr-complex (in C6H6, room temp.); decantation, extn. (C6H6);
DOI:10.1016/S0020-1693(00)95609-3

Reference yield:

: 40545-10-6
(1-diphenylphosphino-2-diphenylarsinoethane)chromium tetracarbonyl

: 59993-11-2
iodo(1-diphenylphosphino-2-diphenylarsinoethane)chromium tetracarbonyl iodide

Guidance literature:: With iodine; In hexane; benzene; N2-atmosphere; dropwise addn. of iodine (in hexane) to Cr-complex (in C6H6, room temp.); elem. anal.;
DOI:10.1016/S0020-1693(00)95609-3