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Technology Process of (Z)-methyl 1,4-dihydro-4-(4-methoxyphenyl)-5'-phenethyl-1,3-diphenyl-2'-(phenylimino)spiro[3H-1,2,4-triazole-5,3'(2'S10H)-thiophene]-4'-carboxylate

(Z)-methyl 1,4-dihydro-4-(4-methoxyphenyl)-5'-phenethyl-1,3-diphenyl-2'-(phenylimino)spiro[3H-1,2,4-triazole-5,3'(2'S10H)-thiophene]-4'-carboxylate

Base Information
  • Chemical Name:(Z)-methyl 1,4-dihydro-4-(4-methoxyphenyl)-5'-phenethyl-1,3-diphenyl-2'-(phenylimino)spiro[3H-1,2,4-triazole-5,3'(2'S10H)-thiophene]-4'-carboxylate
  • CAS No.:1123535-73-8
  • Molecular Formula:C40H34N4O3S
  • Molecular Weight:650.801
  • Hs Code.:
(Z)-methyl 1,4-dihydro-4-(4-methoxyphenyl)-5'-phenethyl-1,3-diphenyl-2'-(phenylimino)spiro[3H-1,2,4-triazole-5,3'(2'S<sub>10</sub>H)-thiophene]-4'-carboxylate

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Chemical Property of (Z)-methyl 1,4-dihydro-4-(4-methoxyphenyl)-5'-phenethyl-1,3-diphenyl-2'-(phenylimino)spiro[3H-1,2,4-triazole-5,3'(2'S10H)-thiophene]-4'-carboxylate
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Technology Process of (Z)-methyl 1,4-dihydro-4-(4-methoxyphenyl)-5'-phenethyl-1,3-diphenyl-2'-(phenylimino)spiro[3H-1,2,4-triazole-5,3'(2'S10H)-thiophene]-4'-carboxylate

There total 1 articles about (Z)-methyl 1,4-dihydro-4-(4-methoxyphenyl)-5'-phenethyl-1,3-diphenyl-2'-(phenylimino)spiro[3H-1,2,4-triazole-5,3'(2'S10H)-thiophene]-4'-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

methyl 5-phenyl-2,3-pentadienoate
1006879-10-2

methyl 5-phenyl-2,3-pentadienoate

C<sub>28</sub>H<sub>22</sub>N<sub>4</sub>OS
1123535-43-2

C28H22N4OS

methyl 1,4-dihydro-4-(4-methoxyphenyl)-5'-phenethyl-1,1',3-triphenyl-2'-thioxospiro[3H-1,2,4-triazole-5,3'(2'H)-pyrrole]-4'-carboxylate
1123535-76-1

methyl 1,4-dihydro-4-(4-methoxyphenyl)-5'-phenethyl-1,1',3-triphenyl-2'-thioxospiro[3H-1,2,4-triazole-5,3'(2'H)-pyrrole]-4'-carboxylate

(Z)-methyl 1,4-dihydro-4-(4-methoxyphenyl)-5'-phenethyl-1,3-diphenyl-2'-(phenylimino)spiro[3H-1,2,4-triazole-5,3'(2'S<sub>10</sub>H)-thiophene]-4'-carboxylate
1123535-73-8

(Z)-methyl 1,4-dihydro-4-(4-methoxyphenyl)-5'-phenethyl-1,3-diphenyl-2'-(phenylimino)spiro[3H-1,2,4-triazole-5,3'(2'S10H)-thiophene]-4'-carboxylate

Guidance literature:
In toluene; at 110 ℃; for 2h; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo802687m
upstream raw materials:

methyl 5-phenyl-2,3-pentadienoate

C28H22N4OS

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