1H-Imidazole-4-carboxaldehyde, 5-methyl-1-(triphenylmethyl)-

Base Information

Chemical Name:1H-Imidazole-4-carboxaldehyde, 5-methyl-1-(triphenylmethyl)-
CAS No.:113140-81-1
Molecular Formula:C24H20N2O
Molecular Weight:352.436
Hs Code.:
Mol file:113140-81-1.mol

Synonyms:5-Methyl-1-trityl-1H-imidazole-4-carbaldehyde;5-methyl-1-(triphenylmethyl)-1H-imidazole-4-carbaldehyde;1-triphenylmethyl-5-methyl-1H-imidazole-4-carboxaldehyde;4-formyl-5-methyl-1-tritylimidazole;5-Methyl-1-triphenylmethyl-1H-imidazole-4-carboxyaldehyde;5-methyl-1-tritylimidazole-4-carboxaldehyde;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Imidazole-4-carboxaldehyde, 5-methyl-1-(triphenylmethyl)-

Chemical Property:

Melting Point:195-196 °C
Boiling Point:516.1±45.0 °C(Predicted)
PSA：34.89000
Density:1.09±0.1 g/cm3(Predicted)
LogP:4.84420

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1H-Imidazole-4-carboxaldehyde, 5-methyl-1-(triphenylmethyl)-

There total 2 articles about 1H-Imidazole-4-carboxaldehyde, 5-methyl-1-(triphenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 68282-53-1
5-methyl-4-formylimidazole

: 76-83-5
trityl chloride

: 113140-81-1
5-methyl-1-(triphenylmethyl)-1H-imidazole-4-carboxaldehyde

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 42h;

Reference yield:

: methanol-dichloromethane

: 33016-47-6
(1-tritylimidazol-4-yl)carboxaldehyde

: 113140-81-1
5-methyl-1-(triphenylmethyl)-1H-imidazole-4-carboxaldehyde

Guidance literature:: With ammonium chloride; In tetrahydrofuran; diethyl ether;

Reference yield: 93.0%

: 6089-04-9
3-(tetrahydropyran-2'-yloxy)propyne

: 113140-81-1
5-methyl-1-(triphenylmethyl)-1H-imidazole-4-carboxaldehyde

: 1008520-77-1
1-(5-methyl-1-trityl-1H-imidazol-4-yl)-4-(tetrahydro-2H-pyran-2-yloxy)but-2-yn-1-ol

Guidance literature:: 3-(tetrahydropyran-2'-yloxy)propyne; With n-butyllithium; In tetrahydrofuran; hexanes; at -78 - 20 ℃; for 0.416667h;

5-methyl-1-(triphenylmethyl)-1H-imidazole-4-carboxaldehyde; In tetrahydrofuran; hexanes; at -78 - 20 ℃; for 1.75h;

With water; In tetrahydrofuran; hexanes; ethyl acetate;