[Ni(CH₂C₆H₅)(C₆H₅P(C₂H₄P(C₆H₅)2)2)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ni(CH₂C₆H₅)(C₆H₅P(C₂H₄P(C₆H₅)2)2)]B(C₆H₅)4

Base Information

• Chemical Name: [Ni(CH₂C₆H₅)(C₆H₅P(C₂H₄P(C₆H₅)2)2)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ni(CH₂C₆H₅)(C₆H₅P(C₂H₄P(C₆H₅)2)2)]B(C₆H₅)4
• CAS No.: 852356-14-0
• Molecular Formula: C₂₄H₂₀B*C₄₁H₄₀NiP₃
• Molecular Weight: 1003.61

Synonyms:

Chemical Property of [Ni(CH₂C₆H₅)(C₆H₅P(C₂H₄P(C₆H₅)2)2)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ni(CH₂C₆H₅)(C₆H₅P(C₂H₄P(C₆H₅)2)2)]B(C₆H₅)4

Chemical Property:

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Safty Information:

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Useful:

Technology Process of [Ni(CH₂C₆H₅)(C₆H₅P(C₂H₄P(C₆H₅)2)2)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ni(CH₂C₆H₅)(C₆H₅P(C₂H₄P(C₆H₅)2)2)]B(C₆H₅)4

There total 1 articles about [Ni(CH₂C₆H₅)(C₆H₅P(C₂H₄P(C₆H₅)2)2)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ni(CH₂C₆H₅)(C₆H₅P(C₂H₄P(C₆H₅)2)2)]B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[bis(2-diphenylphosphinoethyl)phenylphosphine]chloronickel(II) tetraphenylborate (40326-49-6) + benzylmagnesium chloride (6921-34-2) → [Ni(η2-CH2C6H5)(PhP(C2H4PPh2)2)]BPh4 (852356-14-0)

Guidance literature:

In tetrahydrofuran; (N2); Schlenk technique; C6H5CH2MgCl was slowly added to suspn. of Ni complex in THF at -78°C; soln. was stirred overnight; ethanol added dropwise; volatiles removed (vac.); extd. (CH2Cl2); filtered; washed (CH2Cl2); layered with EtOH for several d; filtered; dried (vac.); elem. anal.;

DOI:10.1016/j.jorganchem.2005.01.034

Reference yield:

[Ni(CH2C6H5)(C6H5P(C2H4P(C6H5)2)2)](1+)*B(C6H5)4(1-)=[Ni(CH2C6H5)(C6H5P(C2H4P(C6H5)2)2)]B(C6H5)4 (852356-14-0,75046-68-3) → [NiOS(O)CH2C6H5(C6H5P(C2H4P(C6H5)2)2)](1+)*B(C6H5)4(1-)=[NiOS(O)CH2C6H5(C6H5P(C2H4P(C6H5)2)2)]B(C6H5)4 (75046-75-2)

Guidance literature:

With SO₂; In neat (no solvent); (N2); SO2 condensed onto complex in CO2/acetone bath, warmed slowly to room temp.; dissolved in CH2Cl2, EtOH added, concd. (N2), recrystd. (CH2Cl2/EtOH); elem. anal.;

DOI:10.1016/S0022-328X(00)81236-X

upstream raw materials:

[bis(2-diphenylphosphinoethyl)phenylphosphine]chloronickel(II) tetraphenylborate

benzylmagnesium chloride

Downstream raw materials:

[NiOS(O)CH₂C₆H₅(C₆H₅P(C₂H₄P(C₆H₅)2)2)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[NiOS(O)CH₂C₆H₅(C₆H₅P(C₂H₄P(C₆H₅)2)2)]B(C₆H₅)4

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