1L-(1,2,4/3)-1,3,4-Tri-O-acetyl-2-O-methyl-tetrahydroxy-5-cyclohexen

Base Information

Chemical Name:1L-(1,2,4/3)-1,3,4-Tri-O-acetyl-2-O-methyl-tetrahydroxy-5-cyclohexen
CAS No.:80979-99-3
Molecular Formula:C₁₃H₁₈O₇
Molecular Weight:286.282
Hs Code.:

Synonyms:

Suppliers and Price of 1L-(1,2,4/3)-1,3,4-Tri-O-acetyl-2-O-methyl-tetrahydroxy-5-cyclohexen

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1L-(1,2,4/3)-1,3,4-Tri-O-acetyl-2-O-methyl-tetrahydroxy-5-cyclohexen

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1L-(1,2,4/3)-1,3,4-Tri-O-acetyl-2-O-methyl-tetrahydroxy-5-cyclohexen

There total 5 articles about 1L-(1,2,4/3)-1,3,4-Tri-O-acetyl-2-O-methyl-tetrahydroxy-5-cyclohexen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 642-38-6
quebrachitol

: 80979-99-3
1L-(1,2,4/3)-1,3,4-Tri-O-acetyl-2-O-methyl-tetrahydroxy-5-cyclohexen

Guidance literature:: Multi-step reaction with 5 steps

1: 10 percent / anh. p-toluenesulfonic acid / dimethylformamide / 20 h / 80 °C

2: 96 percent / pyridine

3: 89 percent / tetrahydrofuran; H₂O; acetic acid / 90 °C

4: 78 percent / pyridine; CHCl₃ / 80 °C

5: 1) NaI, Zn-powder / 1) DMF, 130 deg C, 2) pyridine

With toluene-4-sulfonic acid; sodium iodide; zinc; In tetrahydrofuran; pyridine; chloroform; water; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 80971-01-3
1L-1,3,4-Tri-O-acetyl-5,6-O-isopropyliden-2-O-methyl-chiro-inosit

: 80979-99-3
1L-(1,2,4/3)-1,3,4-Tri-O-acetyl-2-O-methyl-tetrahydroxy-5-cyclohexen

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / tetrahydrofuran; H₂O; acetic acid / 90 °C

2: 78 percent / pyridine; CHCl₃ / 80 °C

3: 1) NaI, Zn-powder / 1) DMF, 130 deg C, 2) pyridine

With sodium iodide; zinc; In tetrahydrofuran; pyridine; chloroform; water; acetic acid;

Reference yield:

: 17230-38-5,56193-51-2,96554-71-1
1L-1,3,4-tri-O-acetyl-2-O-methyl-chiro-inositol

: 80979-99-3
1L-(1,2,4/3)-1,3,4-Tri-O-acetyl-2-O-methyl-tetrahydroxy-5-cyclohexen

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / pyridine; CHCl₃ / 80 °C

2: 1) NaI, Zn-powder / 1) DMF, 130 deg C, 2) pyridine

With sodium iodide; zinc; In pyridine; chloroform;