tetraphenylstibonium succinimide

Base Information

• Chemical Name: tetraphenylstibonium succinimide
• CAS No.: 86529-78-4
• Molecular Formula: C₂₈H₂₄NO₂Sb
• Molecular Weight: 528.254
• Mol file: 86529-78-4.mol

Synonyms:

Chemical Property of tetraphenylstibonium succinimide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetraphenylstibonium succinimide

There total 1 articles about tetraphenylstibonium succinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Succinimide (123-56-8,89963-74-6) + tetraphenylantimony(V) bromide (16894-69-2) → tetraphenylstibonium succinimide (86529-78-4,91855-01-5)

Guidance literature:

With (C₂H₅)3N; In benzene; byproducts: Et3N*HBr; soln. of mixt. stirred at room temp. for 3 h, refluxed for 1 h; filtered, concd. (vac.), recrystd. (MeCN/petroleum ether); elem. anal.;

Reference yield:

tetraphenylstibonium succinimide (86529-78-4,91855-01-5) → tetraphenylantimony(V) bromide (16894-69-2)

Guidance literature:

With Br₂; In tetrachloromethane; byproducts: bromosuccinimide; Br2 soln. slowly added to Sb compd. soln. at -5°C for 30 min, allowed to come at room temp.; evapd. (vac.), not isolated, detected by IR, TLC;

Reference yield:

tetraphenylstibonium succinimide (86529-78-4,91855-01-5) → tetraphenylstibonium p-nitrobenzoate (75137-01-8)

Guidance literature:

Multi-step reaction with 2 steps

1: Br₂ / tetrachloromethane

2: benzene

With Br₂; In tetrachloromethane; benzene;

upstream raw materials:

Succinimide

tetraphenylantimony(V) bromide

Downstream raw materials:

tetraphenylantimony(V) bromide

tetraphenylstibonium p-nitrobenzoate