[(PhCH2)2NAlN(CH2Ph)-μ-(CH2C6H4)]2

Base Information

Chemical Name:[(PhCH2)2NAlN(CH2Ph)-μ-(CH2C6H4)]2
CAS No.:281666-91-9
Molecular Formula:C₅₆H₅₄Al₂N₄
Molecular Weight:837.035
Hs Code.:

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Chemical Property of [(PhCH2)2NAlN(CH2Ph)-μ-(CH2C6H4)]2

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Technology Process of [(PhCH2)2NAlN(CH2Ph)-μ-(CH2C6H4)]2

There total 2 articles about [(PhCH2)2NAlN(CH2Ph)-μ-(CH2C6H4)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.1%

: 75-24-1
trimethylaluminum

: 103-49-1
dibenzylamine

: 281666-91-9
[(PhCH2)2NAlN(CH2Ph)-μ-(CH2C6H4)]2

Guidance literature:: In toluene; standard inert-atmosphere technique; dibenzylamine and Me3Al mixed in 2:1 mole ratio at room temp. in high-pressure reaction tube; heated at 155°C for 21-25 d in oil bath; PMR monitoring; solvent removed in vac.; solid washed (hexane); recrystd. (toluene, -15°C);
DOI:10.1021/om000072z

Reference yield:

: 212757-07-8
[MeAlN(CH2Ph)-μ-(CH2C6H4)]2

: 103-49-1
dibenzylamine

: 281666-91-9
[(PhCH2)2NAlN(CH2Ph)-μ-(CH2C6H4)]2

Guidance literature:: standard inert-atmosphere technique; dibenzylamine and AlN-ortho-metalated dimer mixed in 1:1 mole ratio; heated at 155°C;
DOI:10.1021/om000072z