2'-Adenylic acid, N-benzoyl-5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(4-nitrophenyl)ethyl] ester, 3'-benzoate, compd. with N,N-diethylethanamine (1:1)

Base Information

Chemical Name:2'-Adenylic acid, N-benzoyl-5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(4-nitrophenyl)ethyl] ester, 3'-benzoate, compd. with N,N-diethylethanamine (1:1)
CAS No.:113297-64-6
Molecular Formula:C52H45N6O12P.C6H15N
Molecular Weight:1078.13
Hs Code.:

2'-Adenylic acid, N-benzoyl-5'-O-[(4-methoxyphenyl)diphenylmethyl]-,
mono[2-(4-nitrophenyl)ethyl] ester, 3'-benzoate, compd. with
N,N-diethylethanamine (1:1)

Synonyms:

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Chemical Property of 2'-Adenylic acid, N-benzoyl-5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(4-nitrophenyl)ethyl] ester, 3'-benzoate, compd. with N,N-diethylethanamine (1:1)

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Technology Process of 2'-Adenylic acid, N-benzoyl-5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(4-nitrophenyl)ethyl] ester, 3'-benzoate, compd. with N,N-diethylethanamine (1:1)

There total 7 articles about 2'-Adenylic acid, N-benzoyl-5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(4-nitrophenyl)ethyl] ester, 3'-benzoate, compd. with N,N-diethylethanamine (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 93390-26-2
N⁶,3'-Dibenzoyl-5'-O-monomethoxytrityladenosine-2'-(2,5-dichlorophenyl),(2-(4-nitrophenyl)-ethyl)-phosphate

: 121-44-8
triethylamine

: 113297-64-6
N⁶,O^3'-dibenzoyl-5'-O-(4-monomethoxytrityl)-2'-O-[2-(4-nitrophenylethyl)-phosphato]adenosine triethylammonium salt

Guidance literature:: With pyridine; 4-nitrobenzaldehyde oxime; In water; for 0.666667h; Ambient temperature;

Reference yield:

: 69504-00-3
N⁶-Benzoyl-5'-O-(monomethoxytrityl)adenosine

: 113297-64-6
N⁶,O^3'-dibenzoyl-5'-O-(4-monomethoxytrityl)-2'-O-[2-(4-nitrophenylethyl)-phosphato]adenosine triethylammonium salt

Guidance literature:: Multi-step reaction with 4 steps

1: 37 percent / triethylamine / acetonitrile / 12 h / Ambient temperature

2: 37 percent / triethylamine / acetonitrile / 12 h / Ambient temperature

4: 90 percent / p-nitrobenzaldoxime, pyridine / H₂O / 0.67 h / Ambient temperature

With pyridine; triethylamine; 4-nitrobenzaldehyde oxime; In water; acetonitrile;

Reference yield:

: 4546-55-8
N-benzoyladenosine

: 113297-64-6
N⁶,O^3'-dibenzoyl-5'-O-(4-monomethoxytrityl)-2'-O-[2-(4-nitrophenylethyl)-phosphato]adenosine triethylammonium salt

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / pyridine / 5 h / Ambient temperature

2: 37 percent / triethylamine / acetonitrile / 12 h / Ambient temperature

3: 37 percent / triethylamine / acetonitrile / 12 h / Ambient temperature

5: 90 percent / p-nitrobenzaldoxime, pyridine / H₂O / 0.67 h / Ambient temperature

With pyridine; triethylamine; 4-nitrobenzaldehyde oxime; In water; acetonitrile;