O-1-Benzyl-N-benzyloxycarbonyl-γ-L-glutamylamino)-butyryl>-glykolsaeure-<4-nitro-benzylester>

Base Information

Chemical Name:O-1-Benzyl-N-benzyloxycarbonyl-γ-L-glutamylamino)-butyryl>-glykolsaeure-<4-nitro-benzylester>
CAS No.:2830-20-8
Molecular Formula:C₃₃H₃₅N₃O₁₁
Molecular Weight:649.654
Hs Code.:

O-<L-2-(O<sup>1</sup>-Benzyl-N-benzyloxycarbonyl-γ-L-glutamylamino)-butyryl>-glykolsaeure-<4-nitro-benzylester>

Synonyms:

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Chemical Property of O-1-Benzyl-N-benzyloxycarbonyl-γ-L-glutamylamino)-butyryl>-glykolsaeure-<4-nitro-benzylester>

Chemical Property:

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Technology Process of O-1-Benzyl-N-benzyloxycarbonyl-γ-L-glutamylamino)-butyryl>-glykolsaeure-<4-nitro-benzylester>

There total 5 articles about O-1-Benzyl-N-benzyloxycarbonyl-γ-L-glutamylamino)-butyryl>-glykolsaeure-<4-nitro-benzylester> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 619-73-8
4-nitrobenzyl chloride

: 2830-20-8
O-1-Benzyl-N-benzyloxycarbonyl-γ-L-glutamylamino)-butyryl>-glykolsaeure-<4-nitro-benzylester>

Guidance literature:: Multi-step reaction with 4 steps

1: TsOH / toluene / Heating

2: (i) PhSO₂Cl, (ii) /BRN= 2216189/

3: aq. HBr, AcOH

4: (i) ClCO₂iBu, Et₃N, THF, (ii) /BRN= 6714909/

With hydrogen bromide; toluene-4-sulfonic acid; acetic acid; In toluene;
DOI:10.1007/BF00845310

Reference yield:

: 15396-82-4
Glykolsaeure-(4-nitro-benzylester)

: 2830-20-8
O-1-Benzyl-N-benzyloxycarbonyl-γ-L-glutamylamino)-butyryl>-glykolsaeure-<4-nitro-benzylester>

Guidance literature:: Multi-step reaction with 3 steps

1: (i) PhSO₂Cl, (ii) /BRN= 2216189/

2: aq. HBr, AcOH

3: (i) ClCO₂iBu, Et₃N, THF, (ii) /BRN= 6714909/

With hydrogen bromide; acetic acid;
DOI:10.1007/BF00845310

Reference yield:

: 2830-15-1
O--glykolsaeure-(4-nitro-benzylester)

: 2830-20-8
O-1-Benzyl-N-benzyloxycarbonyl-γ-L-glutamylamino)-butyryl>-glykolsaeure-<4-nitro-benzylester>

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HBr, AcOH

2: (i) ClCO₂iBu, Et₃N, THF, (ii) /BRN= 6714909/

With hydrogen bromide; acetic acid;
DOI:10.1007/BF00845310