Technology Process of 3-(3,4,5-trimethoxyphenyl)propyl β-D-glucopyranoside
There total 7 articles about 3-(3,4,5-trimethoxyphenyl)propyl β-D-glucopyranoside which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium methylate;
In
methanol;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: silver carbonate / diethyl ether; dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve
1.2: 14 h / 20 °C / Inert atmosphere; Darkness
2.1: sodium methylate / methanol / 2 h / 20 °C
With
sodium methylate; silver carbonate;
In
methanol; diethyl ether; dichloromethane;
1.1: |Koenigs-Knorr Glycosidation / 1.2: |Koenigs-Knorr Glycosidation;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran
2.1: thionyl chloride / dichloromethane
3.1: potassium carbonate / dimethyl sulfoxide / 6 h / 50 °C
4.1: sodium chloride / dimethyl sulfoxide / 5 h / Reflux
5.1: lithium aluminium tetrahydride / tetrahydrofuran / 2.5 h / 20 °C / Reflux
6.1: silver carbonate / diethyl ether; dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve
6.2: 14 h / 20 °C / Inert atmosphere; Darkness
7.1: sodium methylate / methanol / 2 h / 20 °C
With
lithium aluminium tetrahydride; thionyl chloride; sodium methylate; potassium carbonate; silver carbonate; sodium chloride;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; dimethyl sulfoxide;
6.1: |Koenigs-Knorr Glycosidation / 6.2: |Koenigs-Knorr Glycosidation;
