Technology Process of C14H14FN3O
There total 5 articles about C14H14FN3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 10% palladium on activated carbon; hydrogen; acetic acid / 24 h / 60 °C
2: 1,4-dioxane; water / 16 h / 60 °C
3: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonia; triethylamine / dichloromethane
4: water; trifluoroacetic acid / dichloromethane / 1 h
With
10% palladium on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonia; water; hydrogen; acetic acid; triethylamine; trifluoroacetic acid;
In
1,4-dioxane; dichloromethane; water;
DOI:10.1021/ml100200c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1,4-dioxane; water / 16 h / 60 °C
2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonia; triethylamine / dichloromethane
3: water; trifluoroacetic acid / dichloromethane / 1 h
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonia; water; triethylamine; trifluoroacetic acid;
In
1,4-dioxane; dichloromethane; water;
DOI:10.1021/ml100200c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonia; triethylamine / dichloromethane
2: water; trifluoroacetic acid / dichloromethane / 1 h
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonia; water; triethylamine; trifluoroacetic acid;
In
dichloromethane;
DOI:10.1021/ml100200c
