1-(2-methoxyphenyl)-4-piperazine

Base Information

• Chemical Name: 1-(2-methoxyphenyl)-4-piperazine
• CAS No.: 154744-83-9
• Molecular Formula: C₂₄H₃₃N₃O₂
• Molecular Weight: 395.545

Synonyms:

Chemical Property of 1-(2-methoxyphenyl)-4-piperazine

Chemical Property:

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Technology Process of 1-(2-methoxyphenyl)-4-piperazine

There total 1 articles about 1-(2-methoxyphenyl)-4-piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[5-Methoxy-3,4-dihydro-2H-naphthalen-(1E)-ylidene]-{2-[4-(2-methoxy-phenyl)-piperazin-1-yl]-ethyl}-amine → 1-(2-methoxyphenyl)-4-piperazine (154744-83-9)

Guidance literature:

With sodium tetrahydroborate; In ethanol; for 2h; Yield given; Ambient temperature;

DOI:10.1021/jm00006a013

Reference yield:

1-(2-methoxyphenyl)-4-piperazine (154744-83-9) → 1-(2-methoxyphenyl)-4-{2-[N-(5-methoxy-1,2,3,4-tetrahydronaphthalen-1-yl)methylamino]ethyl}piperazine

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH / CHCl₃ / 1 h

2: LiAlH₄ / tetrahydrofuran / 24 h / Heating

With sodium hydroxide; lithium aluminium tetrahydride; In tetrahydrofuran; chloroform;

DOI:10.1021/jm960087s

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