Acetic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[{(2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-(2-methoxymethoxy-ethylamino)-phosphanyloxymethyl]-tetrahydro-furan-3-yl ester

Base Information

• Chemical Name: Acetic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[{(2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-(2-methoxymethoxy-ethylamino)-phosphanyloxymethyl]-tetrahydro-furan-3-yl ester
• CAS No.: 171973-53-8
• Molecular Formula: C₆₁H₆₂N₁₁O₁₃P
• Molecular Weight: 1188.2

Synonyms:

Chemical Property of Acetic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[{(2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-(2-methoxymethoxy-ethylamino)-phosphanyloxymethyl]-tetrahydro-furan-3-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Acetic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[{(2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-(2-methoxymethoxy-ethylamino)-phosphanyloxymethyl]-tetrahydro-furan-3-yl ester

There total 1 articles about Acetic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[{(2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-(2-methoxymethoxy-ethylamino)-phosphanyloxymethyl]-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-amino-2-(methoxymethoxy)ethane (74264-63-4) + Acetic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-({(2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-diisopropylamino-phosphanyloxymethyl)-tetrahydro-furan-3-yl ester → Acetic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[{(2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-(2-methoxymethoxy-ethylamino)-phosphanyloxymethyl]-tetrahydro-furan-3-yl ester (171973-53-8)

Guidance literature:

With terazole; Multistep reaction; 1.) acetonitrile, 2.) acetonitrile;

DOI:10.1016/00404-0399(50)1384T-

Reference yield:

Acetic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[{(2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-(2-methoxymethoxy-ethylamino)-phosphanyloxymethyl]-tetrahydro-furan-3-yl ester (171973-53-8) → C61H62IN11O13P(1+)*I(1-)

Guidance literature:

With iodine; In acetonitrile;

DOI:10.1016/00404-0399(50)1384T-

Reference yield:

1-amino-2-(methoxymethoxy)ethane (74264-63-4) + Acetic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[{(2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-(2-methoxymethoxy-ethylamino)-phosphanyloxymethyl]-tetrahydro-furan-3-yl ester (171973-53-8) → C27H38N7O10P + C46H54N7O11P

Guidance literature:

With pyridine; iodine; In acetonitrile;

DOI:10.1016/00404-0399(50)1384T-

upstream raw materials:

1-amino-2-(methoxymethoxy)ethane

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