Technology Process of C26H23N3O5S
There total 3 articles about C26H23N3O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
4-methyl-morpholine;
In
dichloromethane;
at 0 ℃;
for 12h;
DOI:10.1002/anie.201505054
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium hydroxide / ethanol / 12 h / Reflux; Molecular sieve
2: thionyl chloride / dichloromethane / 3 h / Reflux
3: 4-methyl-morpholine / dichloromethane / 12 h / 0 °C
With
4-methyl-morpholine; thionyl chloride; potassium hydroxide;
In
ethanol; dichloromethane;
1: |Pfitzinger Quinoline Synthesis;
DOI:10.1002/anie.201505054
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium hydroxide / ethanol / 12 h / Reflux; Molecular sieve
2: thionyl chloride / dichloromethane / 3 h / Reflux
3: 4-methyl-morpholine / dichloromethane / 12 h / 0 °C
With
4-methyl-morpholine; thionyl chloride; potassium hydroxide;
In
ethanol; dichloromethane;
1: |Pfitzinger Quinoline Synthesis;
DOI:10.1002/anie.201505054