(4-(4'-dimethylaminophenyl)pyridine)tungsten pentacarbonyl

Base Information

• Chemical Name: (4-(4'-dimethylaminophenyl)pyridine)tungsten pentacarbonyl
• CAS No.: 906061-18-5
• Molecular Formula: C₁₈H₁₄N₂O₅W
• Molecular Weight: 522.17
• Mol file: 906061-18-5.mol

Synonyms:

Chemical Property of (4-(4'-dimethylaminophenyl)pyridine)tungsten pentacarbonyl

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (4-(4'-dimethylaminophenyl)pyridine)tungsten pentacarbonyl

There total 1 articles about (4-(4'-dimethylaminophenyl)pyridine)tungsten pentacarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + tungsten hexacarbonyl (14040-11-0) + 4-(4-dimethylaminophenyl)pyridine (1137-80-0) → (4-(4'-dimethylaminophenyl)pyridine)tungsten pentacarbonyl (906061-18-5)

Guidance literature:

In tetrahydrofuran; byproducts: CO; (N2); UV irradn. of a soln. of W(CO)6 in THF for 2 h, addn. to a soln. of ligand in THF, stirring at room temp. for 1.5 h; evapn. in vac., chromy. (silica, pentane/CH2Cl2 1:1); elem. anal.;

DOI:10.1039/b601315e

upstream raw materials:

tetrahydrofuran

tungsten hexacarbonyl

4-(4-dimethylaminophenyl)pyridine