2-butyl-1-menthyloxycarbonylpiperidine

Base Information

• Chemical Name: 2-butyl-1-menthyloxycarbonylpiperidine
• CAS No.: 131119-60-3
• Molecular Formula: C₂₀H₃₇NO₂
• Molecular Weight: 323.519
• Mol file: 131119-60-3.mol

Synonyms:

Chemical Property of 2-butyl-1-menthyloxycarbonylpiperidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-butyl-1-menthyloxycarbonylpiperidine

There total 2 articles about 2-butyl-1-menthyloxycarbonylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

n-butyllithium (109-72-8,29786-93-4) + 1-menthyloxycarbonyl-2-methoxypiperidine (131119-56-7,131119-57-8) → 2-butyl-1-menthyloxycarbonylpiperidine (131119-60-3,131119-61-4)

Guidance literature:

With copper(I) bromide dimethylsulfide complex; boron trifluoride diethyl etherate; In diethyl ether; hexane; from -70 deg C to RT;

Reference yield:

1-menthyloxycarbonylpiperidine (131119-62-5) → 2-butyl-1-menthyloxycarbonylpiperidine (131119-60-3,131119-61-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 43 percent / Bu₄NBF₄ / electrochemical oxidation using graphite electrodes

2: 74 percent / CuBr*Me₂S, BF₃*Et₂O / diethyl ether; hexane / from -70 deg C to RT

With copper(I) bromide dimethylsulfide complex; boron trifluoride diethyl etherate; tetrabutylammonium tetrafluoroborate; In diethyl ether; hexane;

upstream raw materials:

n-butyllithium

1-menthyloxycarbonyl-2-methoxypiperidine

1-menthyloxycarbonylpiperidine