C₆₀H₆₉Cl₆N₃O₂₄

Base Information

Chemical Name:C₆₀H₆₉Cl₆N₃O₂₄
CAS No.:178247-96-6
Molecular Formula:C₆₀H₆₉Cl₆N₃O₂₄
Molecular Weight:1428.93
Hs Code.:

C<sub>60</sub>H<sub>69</sub>Cl<sub>6</sub>N<sub>3</sub>O<sub>24</sub>

Synonyms:

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Chemical Property of C₆₀H₆₉Cl₆N₃O₂₄

Chemical Property:

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Technology Process of C₆₀H₆₉Cl₆N₃O₂₄

There total 14 articles about C₆₀H₆₉Cl₆N₃O₂₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98272-33-4
methyl 3-cyclopropylacrylate

: 178247-96-6
C₆₀H₆₉Cl₆N₃O₂₄

Guidance literature:: Multi-step reaction with 11 steps

1: 48 percent / AD-mix-β / 2-methyl-propan-2-ol; H2O / 24 h / Ambient temperature

2: 81 percent / NEt₃ / CH₂Cl₂ / 42 h / 0 °C

3: 100 percent / aq. K₂CO₃ / acetonitrile / 24 h / 50 °C

4: 81 percent / aq. NaN₃, HCO₂Me / methanol / 14 h / 50 °C

5: 96 percent / H₂ / Pd/C / ethyl acetate / 2.5 h / Ambient temperature

6: 96 percent / PPTS / toluene / 1.5 h / 80 °C

7: 100 percent / aq. LiOH / methanol / 1 h / Ambient temperature

8: 100 percent / DCC, DMAP / toluene / 1.4 h / 80 °C

9: 97 percent / HCO₂H / 2 h / Ambient temperature

10: 81 percent / KHCO₃ / tetrahydrofuran / 3 h / Ambient temperature

11: DCC, DMAP / tetrahydrofuran / Ambient temperature

With dmap; lithium hydroxide; formic acid; sodium azide; Methyl formate; AD-mix-β; hydrogen; pyridinium p-toluenesulfonate; potassium carbonate; potassium hydrogencarbonate; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1016/S0960-894X(99)00257-7

Reference yield:

: 178248-34-5,238413-45-1
methyl (2R,3R)-3-cyclopropyl-2,3-epoxypropionate

: 178247-96-6
C₆₀H₆₉Cl₆N₃O₂₄

Guidance literature:: Multi-step reaction with 8 steps

1: 81 percent / aq. NaN₃, HCO₂Me / methanol / 14 h / 50 °C

2: 96 percent / H₂ / Pd/C / ethyl acetate / 2.5 h / Ambient temperature

3: 96 percent / PPTS / toluene / 1.5 h / 80 °C

4: 100 percent / aq. LiOH / methanol / 1 h / Ambient temperature

5: 100 percent / DCC, DMAP / toluene / 1.4 h / 80 °C

6: 97 percent / HCO₂H / 2 h / Ambient temperature

7: 81 percent / KHCO₃ / tetrahydrofuran / 3 h / Ambient temperature

8: DCC, DMAP / tetrahydrofuran / Ambient temperature

With dmap; lithium hydroxide; formic acid; sodium azide; Methyl formate; hydrogen; pyridinium p-toluenesulfonate; potassium hydrogencarbonate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethyl acetate; toluene;
DOI:10.1016/S0960-894X(99)00257-7

Reference yield:

: 178248-33-4
methyl (2S,3R)-3-cyclopropyl-2,3-dihydroxypropionate

: 178247-96-6
C₆₀H₆₉Cl₆N₃O₂₄

Guidance literature:: Multi-step reaction with 10 steps

1: 81 percent / NEt₃ / CH₂Cl₂ / 42 h / 0 °C

2: 100 percent / aq. K₂CO₃ / acetonitrile / 24 h / 50 °C

3: 81 percent / aq. NaN₃, HCO₂Me / methanol / 14 h / 50 °C

4: 96 percent / H₂ / Pd/C / ethyl acetate / 2.5 h / Ambient temperature

5: 96 percent / PPTS / toluene / 1.5 h / 80 °C

6: 100 percent / aq. LiOH / methanol / 1 h / Ambient temperature

7: 100 percent / DCC, DMAP / toluene / 1.4 h / 80 °C

8: 97 percent / HCO₂H / 2 h / Ambient temperature

9: 81 percent / KHCO₃ / tetrahydrofuran / 3 h / Ambient temperature

10: DCC, DMAP / tetrahydrofuran / Ambient temperature

With dmap; lithium hydroxide; formic acid; sodium azide; Methyl formate; hydrogen; pyridinium p-toluenesulfonate; potassium carbonate; potassium hydrogencarbonate; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; toluene; acetonitrile;
DOI:10.1016/S0960-894X(99)00257-7