9-(3-Benzyloxy-propyl)-4b-chloro-5,6,8,9,10,11-hexahydro-4bH-7,12-diaza-cyclonona[a]indene-7,11-dicarboxylic acid 7-benzyl ester 11-methyl ester

Base Information

Chemical Name:9-(3-Benzyloxy-propyl)-4b-chloro-5,6,8,9,10,11-hexahydro-4bH-7,12-diaza-cyclonona[a]indene-7,11-dicarboxylic acid 7-benzyl ester 11-methyl ester
CAS No.:116556-56-0
Molecular Formula:C₃₄H₃₇ClN₂O₅
Molecular Weight:589.131
Hs Code.:

9-(3-Benzyloxy-propyl)-4b-chloro-5,6,8,9,10,11-hexahydro-4bH-7,12-diaza-cyclonona[a]indene-7,11-dicarboxylic acid 7-benzyl ester 11-methyl ester

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Chemical Property of 9-(3-Benzyloxy-propyl)-4b-chloro-5,6,8,9,10,11-hexahydro-4bH-7,12-diaza-cyclonona[a]indene-7,11-dicarboxylic acid 7-benzyl ester 11-methyl ester

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Technology Process of 9-(3-Benzyloxy-propyl)-4b-chloro-5,6,8,9,10,11-hexahydro-4bH-7,12-diaza-cyclonona[a]indene-7,11-dicarboxylic acid 7-benzyl ester 11-methyl ester

There total 9 articles about 9-(3-Benzyloxy-propyl)-4b-chloro-5,6,8,9,10,11-hexahydro-4bH-7,12-diaza-cyclonona[a]indene-7,11-dicarboxylic acid 7-benzyl ester 11-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116527-86-7
3-benzyloxycarbonyl-5-(3-benzyloxypropyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indol-7-carbonsauremethylester

: 116556-56-0
9-(3-Benzyloxy-propyl)-4b-chloro-5,6,8,9,10,11-hexahydro-4bH-7,12-diaza-cyclonona[a]indene-7,11-dicarboxylic acid 7-benzyl ester 11-methyl ester

Guidance literature:: With tert-butylhypochlorite; triethylamine; In tetrachloromethane; dichloromethane; at 0 ℃;
DOI:10.1016/S0040-4020(01)86862-9

Reference yield:

: 116527-78-7,116556-53-7
2-(3-benzyloxypropyl)-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indol-3-on

: 116556-56-0
9-(3-Benzyloxy-propyl)-4b-chloro-5,6,8,9,10,11-hexahydro-4bH-7,12-diaza-cyclonona[a]indene-7,11-dicarboxylic acid 7-benzyl ester 11-methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / Lithium aluminium hydride / tetrahydrofuran / 1 h / Heating

2: 1.) water; / 1.) aceton; 2.) 50 deg C, 1 h

3: 68 percent / HCl / CH₂Cl₂ / 2 h / Ambient temperature

4: triethylamine, tert.-butylhypochlorite / CCl₄; CH₂Cl₂ / 0 °C

With hydrogenchloride; lithium aluminium tetrahydride; tert-butylhypochlorite; water; triethylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane;
DOI:10.1016/S0040-4020(01)86862-9

Reference yield:

: 116527-79-8,116527-80-1
2-(3-benzyloxypropyl)-2,3,5,6,11,11b-hexahydro-1H-indolizino<8,7-b>indol

: 116556-56-0
9-(3-Benzyloxy-propyl)-4b-chloro-5,6,8,9,10,11-hexahydro-4bH-7,12-diaza-cyclonona[a]indene-7,11-dicarboxylic acid 7-benzyl ester 11-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) water; / 1.) aceton; 2.) 50 deg C, 1 h

2: 68 percent / HCl / CH₂Cl₂ / 2 h / Ambient temperature

3: triethylamine, tert.-butylhypochlorite / CCl₄; CH₂Cl₂ / 0 °C

With hydrogenchloride; tert-butylhypochlorite; water; triethylamine; In tetrachloromethane; dichloromethane;
DOI:10.1016/S0040-4020(01)86862-9