Technology Process of C32H40F3I2NO12
There total 10 articles about C32H40F3I2NO12 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
caesium carbonate;
In
dichloromethane;
at 20 ℃;
for 3.5h;
DOI:10.1021/ja205339p
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: hydrazine hydrate / methanol; dichloromethane / 3 h / 20 °C
2.1: caesium carbonate / dichloromethane / 3.5 h / 20 °C
3.1: dichloromethane / -78 - 20 °C / Molecular sieve
3.2: 0.5 h / -78 °C
4.1: triethylamine tris(hydrogen fluoride) / acetonitrile / 20 - 60 °C
5.1: dichloromethane / -50 - 20 °C / Molecular sieve
5.2: 0.5 h / -78 °C
6.1: hydrazine hydrate / methanol; dichloromethane / 3 h / 20 °C
7.1: caesium carbonate / dichloromethane / 3.5 h / 20 °C
With
caesium carbonate; hydrazine hydrate; triethylamine tris(hydrogen fluoride);
In
methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja205339p
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: caesium carbonate / dichloromethane / 3.5 h / 20 °C
2.1: dichloromethane / -78 - 20 °C / Molecular sieve
2.2: 0.5 h / -78 °C
3.1: triethylamine tris(hydrogen fluoride) / acetonitrile / 20 - 60 °C
4.1: dichloromethane / -50 - 20 °C / Molecular sieve
4.2: 0.5 h / -78 °C
5.1: hydrazine hydrate / methanol; dichloromethane / 3 h / 20 °C
6.1: caesium carbonate / dichloromethane / 3.5 h / 20 °C
With
caesium carbonate; hydrazine hydrate; triethylamine tris(hydrogen fluoride);
In
methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja205339p
