C₆₃H₆₃PSi₃

Base Information

Chemical Name:C₆₃H₆₃PSi₃
CAS No.:1556687-09-2
Molecular Formula:C₆₃H₆₃PSi₃
Molecular Weight:935.423
Hs Code.:

C<sub>63</sub>H<sub>63</sub>PSi<sub>3</sub>

Synonyms:

Suppliers and Price of C₆₃H₆₃PSi₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₃H₆₃PSi₃

Chemical Property:

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Technology Process of C₆₃H₆₃PSi₃

There total 3 articles about C₆₃H₆₃PSi₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 18740-66-4
chlorotris(p-methylphenyl)silane

: 1556687-09-2
C₆₃H₆₃PSi₃

Guidance literature:: With alkali phosphide; In 1,2-dimethoxyethane; for 24h; Inert atmosphere; Glovebox; Schlenk technique; Reflux;
DOI:10.1021/cm500102q

Reference yield:

: 106-38-7
para-bromotoluene

: 1556687-09-2
C₆₃H₆₃PSi₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium; iodine / diethyl ether / 4.5 h / Inert atmosphere; Reflux

1.2: 0.5 h / Inert atmosphere; Reflux

2.1: palladium dichloride; hexachloroethane / tetrahydrofuran / 20 °C / Inert atmosphere; Glovebox

3.1: alkali phosphide / 1,2-dimethoxyethane / 24 h / Inert atmosphere; Glovebox; Schlenk technique; Reflux

With hexachloroethane; iodine; magnesium; palladium dichloride; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether;
DOI:10.1021/cm500102q

Reference yield:

: 4620-79-5
tris(p-tolyl)silane

: 1556687-09-2
C₆₃H₆₃PSi₃

Guidance literature:: Multi-step reaction with 2 steps

1: palladium dichloride; hexachloroethane / tetrahydrofuran / 20 °C / Inert atmosphere; Glovebox

2: alkali phosphide / 1,2-dimethoxyethane / 24 h / Inert atmosphere; Glovebox; Schlenk technique; Reflux

With hexachloroethane; palladium dichloride; In tetrahydrofuran; 1,2-dimethoxyethane;
DOI:10.1021/cm500102q