N₁,N₃-bis(2-(4-(2-(allyloxy)ethoxy)phenoxy)ethyl)-5-ferrocenylisophthalamide

Base Information

Chemical Name:N₁,N₃-bis(2-(4-(2-(allyloxy)ethoxy)phenoxy)ethyl)-5-ferrocenylisophthalamide
CAS No.:1262899-05-7
Molecular Formula:C₄₄H₄₈FeN₂O₈
Molecular Weight:788.721
Hs Code.:

N<sub>1</sub>,N<sub>3</sub>-bis(2-(4-(2-(allyloxy)ethoxy)phenoxy)ethyl)-5-ferrocenylisophthalamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N₁,N₃-bis(2-(4-(2-(allyloxy)ethoxy)phenoxy)ethyl)-5-ferrocenylisophthalamide

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Technology Process of N₁,N₃-bis(2-(4-(2-(allyloxy)ethoxy)phenoxy)ethyl)-5-ferrocenylisophthalamide

There total 2 articles about N₁,N₃-bis(2-(4-(2-(allyloxy)ethoxy)phenoxy)ethyl)-5-ferrocenylisophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1262899-08-0
N₁,N₃-bis(2-(4-hydroxyphenoxy)ethyl)-5-ferrocenylisophthalamide

: 50563-72-9
2-(allyloxy)ethyl 4-methylbenzenesulfonate

: 1262899-05-7
N₁,N₃-bis(2-(4-(2-(allyloxy)ethoxy)phenoxy)ethyl)-5-ferrocenylisophthalamide

Guidance literature:: With K₂CO₃; In acetonitrile; Fe complex, CH2CHCH2OC2H4OSO2C6H4CH3 and K2CO3 suspended in MeCN, heatedunder N2 for 60 h; cooled to room temp., filtered, evapd. (vac.), dissolved in CH2Cl2, filtered, dried (MgSO4), evapd. (vac.), chromd. (silica gel, CH2Cl2/MeOH); obtained as oil;
DOI:10.1039/c0ob00458h

Reference yield: 15.0%

: IC₆H₃(CONHC₂H₄OC₆H₄OC₂H₄OCH₂CHCH₂)2

: ferrocene boronic acid

: 1262899-05-7
N₁,N₃-bis(2-(4-(2-(allyloxy)ethoxy)phenoxy)ethyl)-5-ferrocenylisophthalamide

Guidance literature:: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In sodium hydroxide; 1,2-dimethoxyethane; aq. NaOH; other Radiation; B compd. added to DME, IC6H3(CONHC2H4OC6H4OC2H4OCH2CHCH2)2 added, aq. NaOH added, degassed with N2, Pd complex added, subjected to microwave radiation at 150°C for 30 min; dild. with CHCl3 and H2O, the org. layer sepd., washed (H2O), dried (MgSO4), evapd. (vac.), chromd. (silica gel, hexane/EtOAc); obtained as oil;
DOI:10.1039/c0ob00458h

Reference yield: 25.0%

: 1262899-05-7
N₁,N₃-bis(2-(4-(2-(allyloxy)ethoxy)phenoxy)ethyl)-5-ferrocenylisophthalamide

: 3,5-bis-{4-[bis-(4-tert-butyl-phenyl)-phenyl-methyl]-phenylcarbamoyl}-1-methyl-pyridinium; chloride

: [(C₅H₅)Fe(C₅H₄C₆H₃(CONHC₂H₄OC₆H₄OC₂H₄OCH₂CH)2)]*[CH₃C₅H₃N(CONHC₆H₄C(C₆H₄C(CH₃)3)2C₆H₅)2]⁽¹⁺⁾*Cl^(1-)

Guidance literature:: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; Fe complex and CH3C5H3N(CONHC6H4C(C6H4C(CH3)3)2C6H5)2Cl added to dry CH2Cl2, stirred for 30 min under N2, Ru complex added, stirred under a flowof N2 for 16 h; evapd. (vac.), chromd. (silica gel TLC, CH2Cl2/MeOH, then EtOAc);
DOI:10.1039/c0ob00458h