3-(10,10-dimethyl-3,3-dioxido-3-thia-4-azatricyclo[5.2.1.0~1,5~]dec-4-yl)-1-(1-phenylethyl)-4-(2-phenylvinyl)-2-azetidinone

Base Information

Chemical Name:3-(10,10-dimethyl-3,3-dioxido-3-thia-4-azatricyclo[5.2.1.0~1,5~]dec-4-yl)-1-(1-phenylethyl)-4-(2-phenylvinyl)-2-azetidinone
CAS No.:176702-20-8
Molecular Formula:C₂₉H₃₄N₂O₃S
Molecular Weight:490.667
Hs Code.:
Mol file:176702-20-8.mol

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Chemical Property of 3-(10,10-dimethyl-3,3-dioxido-3-thia-4-azatricyclo[5.2.1.0~1,5~]dec-4-yl)-1-(1-phenylethyl)-4-(2-phenylvinyl)-2-azetidinone

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Technology Process of 3-(10,10-dimethyl-3,3-dioxido-3-thia-4-azatricyclo[5.2.1.0~1,5~]dec-4-yl)-1-(1-phenylethyl)-4-(2-phenylvinyl)-2-azetidinone

There total 5 articles about 3-(10,10-dimethyl-3,3-dioxido-3-thia-4-azatricyclo[5.2.1.0~1,5~]dec-4-yl)-1-(1-phenylethyl)-4-(2-phenylvinyl)-2-azetidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 111687-00-4
cinnamylidene-((S)-1-phenyl-ethyl)-amine

: 176702-14-0
((1S,5R,7R)-10,10-Dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-acetyl chloride

: 176702-20-8
(3R,4S)-3-((1S,5R,7R)-10,10-Dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-1-((S)-1-phenyl-ethyl)-4-((E)-styryl)-azetidin-2-one

Guidance literature:: With triethylamine; In dichloromethane; for 15h; Ambient temperature;
DOI:10.1016/0040-4020(96)00193-7

Reference yield: 75.0%

: 176702-14-0
((1S,5R,7R)-10,10-Dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-acetyl chloride

: 154428-59-8
4-phenyl-(1'R)-(1'-phenylethyl)-1-azabuta-1,3-diene

: 176702-20-8
(3R,4S)-3-((1S,5R,7R)-10,10-Dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-1-((R)-1-phenyl-ethyl)-4-((E)-styryl)-azetidin-2-one

Guidance literature:: With triethylamine; In dichloromethane; for 15h; Ambient temperature;
DOI:10.1016/0040-4020(96)00193-7

Reference yield:

: 176702-13-9
((1S,5R,7R)-10,10-Dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-acetic acid

: 176702-20-8
(3R,4S)-3-((1S,5R,7R)-10,10-Dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-1-((S)-1-phenyl-ethyl)-4-((E)-styryl)-azetidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 4 h / Heating

2: 82 percent / Et₃N / CH₂Cl₂ / 15 h / Ambient temperature

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/0040-4020(96)00193-7