Technology Process of (S)-(-)-1-pentyl-4-(2-propenyl)-1-cyclohexene
There total 7 articles about (S)-(-)-1-pentyl-4-(2-propenyl)-1-cyclohexene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
2: 35 percent / potassium bicarbonate, benzonitrile, 30percent hydrogen peroxide / methanol / 24 h / Ambient temperature
3: ammonium nitrate / nitromethane / 4 h / 80 °C
4: 92 percent / pyridine / diethyl ether / 4 h / Ambient temperature
5: 1) cuprous iodide / 1) diethyl ether, hexane, 0 deg C, 10 min 2) diethyl ether, -40 deg C, 2 h
With
pyridine; copper(l) iodide; ammonium nitrate; dihydrogen peroxide; potassium hydrogencarbonate; benzonitrile;
In
methanol; diethyl ether; nitromethane;
DOI:10.1016/S0040-4020(01)86265-7
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 35 percent / potassium bicarbonate, benzonitrile, 30percent hydrogen peroxide / methanol / 24 h / Ambient temperature
2: ammonium nitrate / nitromethane / 4 h / 80 °C
3: 92 percent / pyridine / diethyl ether / 4 h / Ambient temperature
4: 1) cuprous iodide / 1) diethyl ether, hexane, 0 deg C, 10 min 2) diethyl ether, -40 deg C, 2 h
With
pyridine; copper(l) iodide; ammonium nitrate; dihydrogen peroxide; potassium hydrogencarbonate; benzonitrile;
In
methanol; diethyl ether; nitromethane;
DOI:10.1016/S0040-4020(01)86265-7
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 35 percent / potassium bicarbonate, benzonitrile, 30percent hydrogen peroxide / methanol / 24 h / Ambient temperature
2: ammonium nitrate / nitromethane / 4 h / 80 °C
3: 92 percent / pyridine / diethyl ether / 4 h / Ambient temperature
4: 1) cuprous iodide / 1) diethyl ether, hexane, 0 deg C, 10 min 2) diethyl ether, -40 deg C, 2 h
With
pyridine; copper(l) iodide; ammonium nitrate; dihydrogen peroxide; potassium hydrogencarbonate; benzonitrile;
In
methanol; diethyl ether; nitromethane;
DOI:10.1016/S0040-4020(01)86265-7
