6--1,4,8,11-tetraazacyclotetradecane

Base Information

Chemical Name:6--1,4,8,11-tetraazacyclotetradecane
CAS No.:146953-67-5
Molecular Formula:C₁₇H₃₀N₆O₂
Molecular Weight:350.464
Hs Code.:

6-<N-(4-nitrobenzyl)amino>-1,4,8,11-tetraazacyclotetradecane

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6--1,4,8,11-tetraazacyclotetradecane

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Technology Process of 6--1,4,8,11-tetraazacyclotetradecane

There total 3 articles about 6--1,4,8,11-tetraazacyclotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 555-16-8
4-nitrobenzaldehdye

: 146953-65-3
6-amino-1,4,8,11-tetraazacyclotetradecane

: 146953-67-5
6--1,4,8,11-tetraazacyclotetradecane

Guidance literature:: With hydrogenchloride; methanol; sodium cyanoborohydride; for 3h; Ambient temperature;
DOI:10.1021/jo00059a062

Reference yield:

: 4741-99-5
3,7-diazanonane-1,9-diamine

: 146953-67-5
6--1,4,8,11-tetraazacyclotetradecane

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / Heating

2: 1) BH₃*THF, 2) concd. HCl / 1) THF, reflux, 2) H₂O, reflux

3: 75 percent / 1 M HCl/MeOH, NaBH₃CN / 3 h / Ambient temperature

With hydrogenchloride; methanol; borane-THF; sodium cyanoborohydride; In methanol;
DOI:10.1021/jo00059a062

Reference yield:

: 148584-64-9
6-amino-cyclam-5,7-dione

: 146953-67-5
6--1,4,8,11-tetraazacyclotetradecane

Guidance literature:: Multi-step reaction with 2 steps

1: 1) BH₃*THF, 2) concd. HCl / 1) THF, reflux, 2) H₂O, reflux

2: 75 percent / 1 M HCl/MeOH, NaBH₃CN / 3 h / Ambient temperature

With hydrogenchloride; methanol; borane-THF; sodium cyanoborohydride;
DOI:10.1021/jo00059a062