1,3-Propanediamine, N,N'-bis[(2-methoxyphenyl)methylene]-

Base Information

Chemical Name:1,3-Propanediamine, N,N'-bis[(2-methoxyphenyl)methylene]-
CAS No.:114070-54-1
Molecular Formula:C19H22N2O2
Molecular Weight:310.396
Hs Code.:
DSSTox Substance ID:DTXSID00412987

Synonyms:MeSalpr;1,3-Propanediamine, N,N'-bis[(2-methoxyphenyl)methylene]-;114070-54-1;SCHEMBL10947624;SCHEMBL10947628;SCHEMBL18634661;DTXSID00412987;N,N'-bis(methylsalicylidene)-1,3-propylenediamine;N,N-bis(2-methoxybenzylidene)propane-1,3-diamine

Suppliers and Price of 1,3-Propanediamine, N,N'-bis[(2-methoxyphenyl)methylene]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Propanediamine, N,N'-bis[(2-methoxyphenyl)methylene]-

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:310.168127949
Heavy Atom Count:23
Complexity:336

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC=C1C=NCCCN=CC2=CC=CC=C2OC

Technology Process of 1,3-Propanediamine, N,N'-bis[(2-methoxyphenyl)methylene]-

There total 11 articles about 1,3-Propanediamine, N,N'-bis[(2-methoxyphenyl)methylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.19%

: 109-76-2,54018-94-9
Trimethylenediamine

: 135-02-4
ortho-anisaldehyde

: 114070-54-1
N,N'-bis(2-methoxybenzylidene)propane-1,3-diamine

Guidance literature:: In benzene; for 24h; Heating;

Reference yield:

: 1806-29-7
2,2'-dihydroxybiphenyl

: 114070-54-1
N,N'-bis(2-methoxybenzylidene)propane-1,3-diamine

Guidance literature:: Multi-step reaction with 7 steps

1: 98 percent / K₂CO₃ / acetone / 8 h / Heating

2: 93 percent / decahydronaphthalene / 24 h / 189 °C

3: 78 percent / t-BuOK / dimethylsulfoxide / 18 h / 60 °C

4: O₃ / methanol; CH₂Cl₂ / -70 °C

5: Me₂S / methanol; CH₂Cl₂ / -70 °C

6: 85 percent / NaOH, TEBA / CH₂Cl₂; H₂O / 2 h / Ambient temperature

7: ethanol / 25 °C

With sodium hydroxide; dimethylsulfide; potassium tert-butylate; N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; ozone; In methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; acetone; decalin;

Reference yield:

: 72216-56-9
3,3'-diallyl-2,2'-dihydroxy-1,1'biphenyl

: 114070-54-1
N,N'-bis(2-methoxybenzylidene)propane-1,3-diamine

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / t-BuOK / dimethylsulfoxide / 18 h / 60 °C

2: O₃ / methanol; CH₂Cl₂ / -70 °C

3: Me₂S / methanol; CH₂Cl₂ / -70 °C

4: 85 percent / NaOH, TEBA / CH₂Cl₂; H₂O / 2 h / Ambient temperature

5: ethanol / 25 °C

With sodium hydroxide; dimethylsulfide; potassium tert-butylate; N-benzyl-N,N,N-triethylammonium chloride; ozone; In methanol; ethanol; dichloromethane; water; dimethyl sulfoxide;