cyclopentyloxy-acetic acid 2-(4-methanesulfonyl-phenyl)-1,1-dimethyl-2-oxo-ethyl ester

Base Information

• Chemical Name: cyclopentyloxy-acetic acid 2-(4-methanesulfonyl-phenyl)-1,1-dimethyl-2-oxo-ethyl ester
• CAS No.: 246869-09-0
• Molecular Formula: C₁₈H₂₄O₆S
• Molecular Weight: 368.451
• Mol file: 246869-09-0.mol

Synonyms:

Chemical Property of cyclopentyloxy-acetic acid 2-(4-methanesulfonyl-phenyl)-1,1-dimethyl-2-oxo-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cyclopentyloxy-acetic acid 2-(4-methanesulfonyl-phenyl)-1,1-dimethyl-2-oxo-ethyl ester

There total 5 articles about cyclopentyloxy-acetic acid 2-(4-methanesulfonyl-phenyl)-1,1-dimethyl-2-oxo-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Cyclopentanol (96-41-3) → cyclopentyloxy-acetic acid 2-(4-methanesulfonyl-phenyl)-1,1-dimethyl-2-oxo-ethyl ester (246869-09-0)

Guidance literature:

Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran

2: CMC, DMAP / CH₂Cl₂

With dmap; sodium hydride; In tetrahydrofuran; dichloromethane;

DOI:10.1016/S0960-894X(99)00365-0

Reference yield:

methyl-phenyl-thioether (100-68-5) → cyclopentyloxy-acetic acid 2-(4-methanesulfonyl-phenyl)-1,1-dimethyl-2-oxo-ethyl ester (246869-09-0)

Guidance literature:

Multi-step reaction with 4 steps

1: AlCl₃ / cyclohexane

2: NaOH, Aliquot 336 / toluene; CCl₄

3: Oxone

4: CMC, DMAP / CH₂Cl₂

With dmap; Oxone; sodium hydroxide; aluminium trichloride; Aliquat 336; In tetrachloromethane; dichloromethane; cyclohexane; toluene;

DOI:10.1016/S0960-894X(99)00365-0

Reference yield:

2-methyl-1-(4-(methylthio)phenyl)-propan-1-one (53207-58-2) → cyclopentyloxy-acetic acid 2-(4-methanesulfonyl-phenyl)-1,1-dimethyl-2-oxo-ethyl ester (246869-09-0)

Guidance literature:

Multi-step reaction with 3 steps

1: NaOH, Aliquot 336 / toluene; CCl₄

2: Oxone

3: CMC, DMAP / CH₂Cl₂

With dmap; Oxone; sodium hydroxide; Aliquat 336; In tetrachloromethane; dichloromethane; toluene;

DOI:10.1016/S0960-894X(99)00365-0

upstream raw materials:

(cyclopentyloxy)acetic acid

2-hydroxy-2-methyl-1-(4-(methylsulfonyl)-phenyl)propan-1-one

Cyclopentanol

methyl-phenyl-thioether

Refernces