C₄₇H₄₇ClF₃N₅O₆S₃

Base Information

Chemical Name:C₄₇H₄₇ClF₃N₅O₆S₃
CAS No.:1616557-75-5
Molecular Formula:C₄₇H₄₇ClF₃N₅O₆S₃
Molecular Weight:966.566
Hs Code.:

C<sub>47</sub>H<sub>47</sub>ClF<sub>3</sub>N<sub>5</sub>O<sub>6</sub>S<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₄₇ClF₃N₅O₆S₃

Chemical Property:

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Technology Process of C₄₇H₄₇ClF₃N₅O₆S₃

There total 6 articles about C₄₇H₄₇ClF₃N₅O₆S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616558-02-1
C₁₇H₂₂N₂O₂

: 1616557-75-5
C₄₇H₄₇ClF₃N₅O₆S₃

Guidance literature:: Multi-step reaction with 4 steps

1: lithium hexamethyldisilazane; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / -78 °C

2: sodium carbonate / toluene / Reflux

3: trifluoroacetic acid

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane

With dmap; N,N,N,N,-tetramethylethylenediamine; sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2014.05.036

Reference yield:

: 59247-47-1
tert-butyl-4-bromobenzoate

: 1616557-75-5
C₄₇H₄₇ClF₃N₅O₆S₃

Guidance literature:: Multi-step reaction with 5 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; tert-butyl XPhos / N,N-dimethyl-formamide / 90 °C

2: lithium hexamethyldisilazane; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / -78 °C

3: sodium carbonate / toluene / Reflux

4: trifluoroacetic acid

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane

With dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N,N,N,N,-tetramethylethylenediamine; sodium carbonate; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; lithium hexamethyldisilazane; tert-butyl XPhos; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2014.05.036

Reference yield:

: 1627704-45-3
C₂₄H₂₇BrN₂O₂

: 1616557-75-5
C₄₇H₄₇ClF₃N₅O₆S₃

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / toluene / Reflux

2: trifluoroacetic acid

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane

With dmap; sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane; toluene;
DOI:10.1016/j.bmcl.2014.05.036