Technology Process of C26H40O7
There total 10 articles about C26H40O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran
2: acetic acid
3: pyridine / dichloromethane / -80 °C
4: pyridinium p-toluenesulfonate / dichloromethane
5: water; potassium carbonate / methanol
7: sodium hydride / tetrahydrofuran / 0 - 20 °C
8: diethyl ether / 0 °C
With
pyridine; water; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; acetic acid;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane;
6: Swern oxidation / 7: Wittig-Horner olefination;
DOI:10.1016/j.cclet.2010.11.023
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridinium p-toluenesulfonate / dichloromethane
2: water; potassium carbonate / methanol
4: sodium hydride / tetrahydrofuran / 0 - 20 °C
5: diethyl ether / 0 °C
With
water; pyridinium p-toluenesulfonate; sodium hydride; potassium carbonate;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane;
3: Swern oxidation / 4: Wittig-Horner olefination;
DOI:10.1016/j.cclet.2010.11.023
- Guidance literature:
-
Multi-step reaction with 4 steps
1: water; potassium carbonate / methanol
3: sodium hydride / tetrahydrofuran / 0 - 20 °C
4: diethyl ether / 0 °C
With
water; sodium hydride; potassium carbonate;
In
tetrahydrofuran; methanol; diethyl ether;
2: Swern oxidation / 3: Wittig-Horner olefination;
DOI:10.1016/j.cclet.2010.11.023