(CH₃)3CC₆H₄C₉H₅CH(CH₃)2Si(CH₃)2C₁₂H₉(CH₃)(C₆H₄C(CH₃)3)

Base Information

Chemical Name:(CH₃)3CC₆H₄C₉H₅CH(CH₃)2Si(CH₃)2C₁₂H₉(CH₃)(C₆H₄C(CH₃)3)
CAS No.:1341198-18-2
Molecular Formula:C₄₇H₅₆Si
Molecular Weight:649.047
Hs Code.:

(CH<sub>3</sub>)3CC<sub>6</sub>H<sub>4</sub>C<sub>9</sub>H<sub>5</sub>CH(CH<sub>3</sub>)2Si(CH<sub>3</sub>)2C<sub>12</sub>H<sub>9</sub>(CH<sub>3</sub>)(C<sub>6</sub>H<sub>4</sub>C(CH<sub>3</sub>)3)

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Chemical Property of (CH₃)3CC₆H₄C₉H₅CH(CH₃)2Si(CH₃)2C₁₂H₉(CH₃)(C₆H₄C(CH₃)3)

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Technology Process of (CH₃)3CC₆H₄C₉H₅CH(CH₃)2Si(CH₃)2C₁₂H₉(CH₃)(C₆H₄C(CH₃)3)

There total 6 articles about (CH₃)3CC₆H₄C₉H₅CH(CH₃)2Si(CH₃)2C₁₂H₉(CH₃)(C₆H₄C(CH₃)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 852160-00-0
4-(4-tert-butylphenyl)-2-methyl-3,5,6,7-tetrahydro-s-indacen-1(2H)-one

: 1341198-18-2
(CH₃)3CC₆H₄C₉H₅CH(CH₃)2Si(CH₃)2C₁₂H₉(CH₃)(C₆H₄C(CH₃)3)

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / diethyl ether; benzene / 1 h / Inert atmosphere; Reflux

3.1: n-butyllithium / diethyl ether; hexane / 3 h / -78 - 0 °C / Inert atmosphere

3.2: 5 h / -70 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; toluene-4-sulfonic acid; In diethyl ether; hexane; benzene;
DOI:10.1021/om200610b

Reference yield:

: 656800-67-8
4-bromo-2-methyl-3,5,6,7-tetrahydro-s-indacen-1(2H)-one

: 1341198-18-2
(CH₃)3CC₆H₄C₉H₅CH(CH₃)2Si(CH₃)2C₁₂H₉(CH₃)(C₆H₄C(CH₃)3)

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium diacetate; sodium carbonate; triphenylphosphine / 1,2-dimethoxyethane; water / 6 h / Inert atmosphere; Reflux

2.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: toluene-4-sulfonic acid / diethyl ether; benzene / 1 h / Inert atmosphere; Reflux

4.1: n-butyllithium / diethyl ether; hexane / 3 h / -78 - 0 °C / Inert atmosphere

4.2: 5 h / -70 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; palladium diacetate; sodium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In 1,2-dimethoxyethane; diethyl ether; hexane; water; benzene; 1.1: Suzuki coupling;
DOI:10.1021/om200610b

Reference yield:

: C₂₃H₂₈O

: 1341198-18-2
(CH₃)3CC₆H₄C₉H₅CH(CH₃)2Si(CH₃)2C₁₂H₉(CH₃)(C₆H₄C(CH₃)3)

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / diethyl ether; benzene / 1 h / Inert atmosphere; Reflux

2.1: n-butyllithium / diethyl ether; hexane / 3 h / -78 - 0 °C / Inert atmosphere

2.2: 5 h / -70 - 20 °C / Inert atmosphere

With n-butyllithium; toluene-4-sulfonic acid; In diethyl ether; hexane; benzene;
DOI:10.1021/om200610b