Diazo bis-(4-chloro-phenyl)-methane

Base Information

Chemical Name:Diazo bis-(4-chloro-phenyl)-methane
CAS No.:1143-92-6
Molecular Formula:C13H8Cl2N2
Molecular Weight:263.126
Hs Code.:
DSSTox Substance ID:DTXSID60462382
Nikkaji Number:J259.276B
Wikidata:Q82286911
Mol file:1143-92-6.mol

Synonyms:diazo bis-(4-chloro-phenyl)-methane;1143-92-6;di(p-chlorophenyl)diazomethane;di(4-chlorophenyl)diazomethane;SCHEMBL7787764;DTXSID60462382;RBYYFMWIKIJOTA-UHFFFAOYSA-N

Suppliers and Price of Diazo bis-(4-chloro-phenyl)-methane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Diazo bis-(4-chloro-phenyl)-methane

Chemical Property:

XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:262.0064537
Heavy Atom Count:17
Complexity:273

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C(=[N+]=[N-])C2=CC=C(C=C2)Cl)Cl

Technology Process of Diazo bis-(4-chloro-phenyl)-methane

There total 4 articles about Diazo bis-(4-chloro-phenyl)-methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 5463-11-6
4,4'-dichlorobenzophenone hydrazone

: 1143-92-6
bis-(4-chlorophenyl)diazomethane

Guidance literature:: With sodium sulfate; potassium hydroxide; mercury(II) oxide; In tetrahydrofuran; ethanol; Darkness;
DOI:10.1016/j.tetlet.2011.01.116

Reference yield: 93.0%

: C₂₂H₂₀Cl₂N₂O₂S

: 1143-92-6
bis-(4-chlorophenyl)diazomethane

Guidance literature:: With N,N,N',N'-tetramethylguanidine; In dichloromethane; formamide; at 75 ℃;
DOI:10.1002/anie.201608444

Reference yield:

: 90-98-2
4,4'-Dichlorobenzophenone

: 1143-92-6
bis-(4-chlorophenyl)diazomethane

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; hydrazine hydrate / 180 °C

2: benzene; HgO

With ethanol; hydrazine hydrate; mercury(II) oxide; benzene;
DOI:10.1039/jr9330000406