2,3-dichlorobicyclo-[2.2.1]hept-5-ene-2,3-dicardicarboxylic acid N-m-carboxyphenylimide

Base Information

• Chemical Name: 2,3-dichlorobicyclo-[2.2.1]hept-5-ene-2,3-dicardicarboxylic acid N-m-carboxyphenylimide
• CAS No.: 1380423-11-9
• Molecular Formula: C₁₆H₁₁Cl₂NO₄
• Molecular Weight: 352.174
• Mol file: 1380423-11-9.mol

Synonyms:

Chemical Property of 2,3-dichlorobicyclo-[2.2.1]hept-5-ene-2,3-dicardicarboxylic acid N-m-carboxyphenylimide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-dichlorobicyclo-[2.2.1]hept-5-ene-2,3-dicardicarboxylic acid N-m-carboxyphenylimide

There total 3 articles about 2,3-dichlorobicyclo-[2.2.1]hept-5-ene-2,3-dicardicarboxylic acid N-m-carboxyphenylimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

dichloromaleic acid N-m-carboxyphenylimide (65833-19-4) + cyclopenta-1,3-diene (542-92-7,25568-84-7,7313-32-8) → 2,3-dichlorobicyclo-[2.2.1]hept-5-ene-2,3-dicardicarboxylic acid N-m-carboxyphenylimide (1380423-11-9)

Guidance literature:

In benzene; at 40 ℃; for 4.25h;

DOI:10.1134/S1070428012020248

Reference yield:

C11H7Cl2NO5 → 2,3-dichlorobicyclo-[2.2.1]hept-5-ene-2,3-dicardicarboxylic acid N-m-carboxyphenylimide (1380423-11-9)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / 2 h / 80 - 108 °C

2: benzene / 4.25 h / 40 °C

With acetic acid; In benzene;

DOI:10.1134/S1070428012020248

Reference yield:

meta-aminobenzoic acid (99-05-8,159139-79-4) → 2,3-dichlorobicyclo-[2.2.1]hept-5-ene-2,3-dicardicarboxylic acid N-m-carboxyphenylimide (1380423-11-9)

Guidance literature:

Multi-step reaction with 3 steps

1: acetic acid / 2 h / 80 - 108 °C

2: acetic acid / 2 h / 80 - 108 °C

3: benzene / 4.25 h / 40 °C

With acetic acid; In acetic acid; benzene;

DOI:10.1134/S1070428012020248

upstream raw materials:

dichloromaleic acid N-m-carboxyphenylimide

cyclopenta-1,3-diene

meta-aminobenzoic acid

Refernces