Technology Process of C39H59NO4Si2
There total 3 articles about C39H59NO4Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(1S)-10-camphorsulfonic acid;
In
dichloromethane;
at 70 ℃;
for 3h;
optical yield given as %de;
diastereoselective reaction;
Inert atmosphere;
DOI:10.1021/jo202179s
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 24 h / 35 °C / Inert atmosphere
2: (1S)-10-camphorsulfonic acid / dichloromethane / 3 h / 70 °C / Inert atmosphere
With
Hoveyda-Grubbs catalyst second generation; (1S)-10-camphorsulfonic acid;
In
dichloromethane;
DOI:10.1021/jo202179s
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 24 h / 35 °C / Inert atmosphere
2: (1S)-10-camphorsulfonic acid / dichloromethane / 3 h / 70 °C / Inert atmosphere
With
Hoveyda-Grubbs catalyst second generation; (1S)-10-camphorsulfonic acid;
In
dichloromethane;
DOI:10.1021/jo202179s