(η1,η2-methoxycyclooct-5-enyl)(2-(bis(2-methoxyphenyl)phosphonium)benzenesulfonate)palladium(II)

Base Information

Chemical Name:(η1,η2-methoxycyclooct-5-enyl)(2-(bis(2-methoxyphenyl)phosphonium)benzenesulfonate)palladium(II)
CAS No.:1007117-72-7
Molecular Formula:C₂₉H₃₃O₆PPdS
Molecular Weight:647.037
Hs Code.:

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Chemical Property of (η1,η2-methoxycyclooct-5-enyl)(2-(bis(2-methoxyphenyl)phosphonium)benzenesulfonate)palladium(II)

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Technology Process of (η1,η2-methoxycyclooct-5-enyl)(2-(bis(2-methoxyphenyl)phosphonium)benzenesulfonate)palladium(II)

There total 1 articles about (η1,η2-methoxycyclooct-5-enyl)(2-(bis(2-methoxyphenyl)phosphonium)benzenesulfonate)palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: {Pd(μ-chloro)(σ,π-8-methoxy-cycloocten-1-yl)}2

: 257290-43-0
2-{bis(2-methoxyphenyl)phosphino}benzenesulphonic acid

: 1007117-72-7
(η1,η2-methoxycyclooct-5-enyl)(2-(bis(2-methoxyphenyl)phosphonium)benzenesulfonate)palladium(II)

Guidance literature:: With NaH; In dichloromethane; under N2; NaH reacted with ligand in CH2Cl2 at room temp. for 30 min; soln. of Pd complex in CH2Cl2 added; stirred at room temp. for 1 h; concd.; n-pentane added; filtered; ppt. washed with n-pentane; elem. anal.;
DOI:10.1039/b711280g

Reference yield: 40.0%

: 1007117-72-7
(η1,η2-methoxycyclooct-5-enyl)(2-(bis(2-methoxyphenyl)phosphonium)benzenesulfonate)palladium(II)

: 853942-19-5
bis(2-(bis(2-methoxyphenyl)phosphonium)benzenesulfonate)palladium(II)

Guidance literature:: In methanol; under N2; Pd complex dissolved in MeOH; heated to 90°C for 2 h; cooled slowly to room temp.; Pd complex and Pd black obtained; decanted; filtered; washed with n-pentane; elem. anal.;
DOI:10.1039/b711280g