(Z)-(4-fluorobut-1-ene-1,4-diyl)dibenzene

Base Information

Chemical Name:(Z)-(4-fluorobut-1-ene-1,4-diyl)dibenzene
CAS No.:1616348-69-6
Molecular Formula:C₁₆H₁₅F
Molecular Weight:226.294
Hs Code.:

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Chemical Property of (Z)-(4-fluorobut-1-ene-1,4-diyl)dibenzene

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Technology Process of (Z)-(4-fluorobut-1-ene-1,4-diyl)dibenzene

There total 3 articles about (Z)-(4-fluorobut-1-ene-1,4-diyl)dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129215-15-2
(Z)-1,4-diphenyl-but-3-en-1-ol

: 1616348-69-6
(Z)-(4-fluorobut-1-ene-1,4-diyl)dibenzene

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at -78 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja505136j

Reference yield:

: 4440-01-1
lithium phenylacetylide

: 1616348-69-6
(Z)-(4-fluorobut-1-ene-1,4-diyl)dibenzene

Guidance literature:: Multi-step reaction with 3 steps

1: lithium perchlorate / tetrahydrofuran / 24 h / 0 °C / Inert atmosphere

2: rosenmund catalyst; hydrogen / ethyl acetate / 2 h / 20 °C / 760.05 Torr / Inert atmosphere

3: diethylamino-sulfur trifluoride / dichloromethane / 12 h / -78 - 20 °C / Inert atmosphere

With diethylamino-sulfur trifluoride; rosenmund catalyst; hydrogen; lithium perchlorate; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1021/ja505136j

Reference yield:

: 96-09-3
styrene oxide

: 1616348-69-6
(Z)-(4-fluorobut-1-ene-1,4-diyl)dibenzene

Guidance literature:: Multi-step reaction with 3 steps

1: lithium perchlorate / tetrahydrofuran / 24 h / 0 °C / Inert atmosphere

2: rosenmund catalyst; hydrogen / ethyl acetate / 2 h / 20 °C / 760.05 Torr / Inert atmosphere

3: diethylamino-sulfur trifluoride / dichloromethane / 12 h / -78 - 20 °C / Inert atmosphere

With diethylamino-sulfur trifluoride; rosenmund catalyst; hydrogen; lithium perchlorate; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1021/ja505136j