Technology Process of C14H24OSi
There total 1 articles about C14H24OSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(1,5-cyclooctadiene)(methoxy)iridium(I) dimer;
In
tetrahydrofuran;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/ja1086547
- Guidance literature:
-
Multi-step reaction with 2 steps
1: norborn-2-ene; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 1,10-Phenanthroline / tetrahydrofuran / 17 h / 100 °C / Inert atmosphere
2: dihydrogen peroxide; potassium hydrogencarbonate / tetrahydrofuran; methanol; water / 40 °C
With
norborn-2-ene; 1,10-Phenanthroline; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; dihydrogen peroxide; potassium hydrogencarbonate;
In
tetrahydrofuran; methanol; water;
2: Tamao-Fleming oxidation;
DOI:10.1021/ja1086547
- Guidance literature:
-
Multi-step reaction with 3 steps
1: norborn-2-ene; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 1,10-Phenanthroline / tetrahydrofuran / 17 h / 100 °C / Inert atmosphere
2: dihydrogen peroxide; potassium hydrogencarbonate / tetrahydrofuran; methanol; water / 40 °C
3: 1H-imidazole / N,N-dimethyl-formamide / 17 h / 20 °C
With
1H-imidazole; norborn-2-ene; 1,10-Phenanthroline; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; dihydrogen peroxide; potassium hydrogencarbonate;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
2: Tamao-Fleming oxidation;
DOI:10.1021/ja1086547
