H-D-Glu-NH2*HCl

Base Information

Chemical Name:H-D-Glu-NH2*HCl
CAS No.:130457-46-4
Molecular Formula:C₂₁H₃₃N₅O₅*ClH
Molecular Weight:471.984
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of H-D-Glu-NH2*HCl

Chemical Property:

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Technology Process of H-D-Glu-NH2*HCl

There total 3 articles about H-D-Glu-NH2*HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 130457-45-3
Boc-D-Glu-NH2

: 130457-46-4
H-D-Glu-NH2*HCl

Guidance literature:: With hydrogenchloride; acetic acid; for 0.333333h;
DOI:10.1016/S0040-4020(01)86764-8

Reference yield:

: 55227-02-6
Boc-D-Glu(OSu)-NH₂

: 130457-46-4
H-D-Glu-NH2*HCl

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / TEA / 1,2-dimethoxy-ethane; H₂O / Ambient temperature

2: 96 percent / AcOH, 1.8N HCl / 0.33 h

With hydrogenchloride; TEA; acetic acid; In 1,2-dimethoxyethane; water;
DOI:10.1016/S0040-4020(01)86764-8

Reference yield:

: 66397-86-2
H-Lys(Z)-NHEt

: 130457-46-4
H-D-Glu-NH2*HCl

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / TEA / 1,2-dimethoxy-ethane; H₂O / Ambient temperature

2: 96 percent / AcOH, 1.8N HCl / 0.33 h

With hydrogenchloride; TEA; acetic acid; In 1,2-dimethoxyethane; water;
DOI:10.1016/S0040-4020(01)86764-8