Technology Process of C17H20O
There total 3 articles about C17H20O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
1.2: 20 h / 20 °C / Inert atmosphere
2.1: diisobutylaluminium hydride / toluene / 4 h / -78 - 0 °C / Inert atmosphere
3.1: ammonium chloride; indium / water; methanol / 12 h / 20 °C / Inert atmosphere
4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 h / 20 °C / Inert atmosphere
With
indium; diisobutylaluminium hydride; sodium hydrogencarbonate; ammonium chloride; Dess-Martin periodane; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1021/ja4025963
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diisobutylaluminium hydride / toluene / 4 h / -78 - 0 °C / Inert atmosphere
2: ammonium chloride; indium / water; methanol / 12 h / 20 °C / Inert atmosphere
3: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 h / 20 °C / Inert atmosphere
With
indium; diisobutylaluminium hydride; sodium hydrogencarbonate; ammonium chloride; Dess-Martin periodane;
In
methanol; dichloromethane; water; toluene;
DOI:10.1021/ja4025963
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium chloride; indium / water; methanol / 12 h / 20 °C / Inert atmosphere
2: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 20 h / 20 °C / Inert atmosphere
With
indium; sodium hydrogencarbonate; ammonium chloride; Dess-Martin periodane;
In
methanol; dichloromethane; water;
DOI:10.1021/ja4025963