p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-iodomethyl-3-cephem-4-carboxylate

Base Information

Chemical Name:p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-iodomethyl-3-cephem-4-carboxylate
CAS No.:131580-92-2
Molecular Formula:C₅₇H₅₀IN₅O₈S₂
Molecular Weight:1124.09
Hs Code.:

p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-iodomethyl-3-cephem-4-carboxylate

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Chemical Property of p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-iodomethyl-3-cephem-4-carboxylate

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Technology Process of p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-iodomethyl-3-cephem-4-carboxylate

There total 1 articles about p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-iodomethyl-3-cephem-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127800-40-2
p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-chloromethyl-3-cephem-4-carboxylate

: 131580-92-2
p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-iodomethyl-3-cephem-4-carboxylate

Guidance literature:: With sodium iodide; In acetone; for 1h;
DOI:10.1248/cpb.38.2271

Reference yield:

: 131580-92-2
p-Methoxybenzyl 7-<(Z)-2-(2-tritylaminothiazol-4-yl)-2-(1-diphenylmethoxycarbonyl-1-methyl)ethoxyiminoacetamido>-3-iodomethyl-3-cephem-4-carboxylate

: 131580-94-4
C₂₂H₂₁N₆O₈S₂^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1: ethyl acetate / 3 h / Ambient temperature

2: CF₃COOH, anisole, NaHCO₃ / 1 h / 0 °C

With sodium hydrogencarbonate; methoxybenzene; trifluoroacetic acid; In ethyl acetate;
DOI:10.1248/cpb.38.2271