Technology Process of C12H7ClIN3O
There total 1 articles about C12H7ClIN3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 90 °C
2: tetraphosphorus decasulfide; sulfur / pyridine / 225 °C
3: potassium tert-butylate / tert-butyl alcohol / 20 °C
4: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 150 °C
5: sulfuric acid / 60 °C
With
tetrakis(triphenylphosphine) palladium(0); tetraphosphorus decasulfide; sulfuric acid; potassium tert-butylate; sulfur; N-ethyl-N,N-diisopropylamine;
In
pyridine; dimethyl sulfoxide; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2013.03.100
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 90 °C
2: tetraphosphorus decasulfide; sulfur / pyridine / 225 °C
3: potassium tert-butylate / tert-butyl alcohol / 20 °C
4: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 150 °C
5: sulfuric acid / 60 °C
With
tetrakis(triphenylphosphine) palladium(0); tetraphosphorus decasulfide; sulfuric acid; potassium tert-butylate; sulfur; N-ethyl-N,N-diisopropylamine;
In
pyridine; dimethyl sulfoxide; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2013.03.100