2-[(2R,3S,4S)-4-Hydroxy-3-((3E,7E)-(R)-5-hydroxy-4,8,12-trimethyl-trideca-3,7,11-trienyl)-3,4-dimethyl-2-(3-trityloxy-propyl)-cyclohex-(Z)-ylidene]-propionaldehyde

Base Information

• Chemical Name: 2-[(2R,3S,4S)-4-Hydroxy-3-((3E,7E)-(R)-5-hydroxy-4,8,12-trimethyl-trideca-3,7,11-trienyl)-3,4-dimethyl-2-(3-trityloxy-propyl)-cyclohex-(Z)-ylidene]-propionaldehyde
• CAS No.: 219753-50-1
• Molecular Formula: C₄₉H₆₄O₄
• Molecular Weight: 717.045

Synonyms:

Chemical Property of 2-[(2R,3S,4S)-4-Hydroxy-3-((3E,7E)-(R)-5-hydroxy-4,8,12-trimethyl-trideca-3,7,11-trienyl)-3,4-dimethyl-2-(3-trityloxy-propyl)-cyclohex-(Z)-ylidene]-propionaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-[(2R,3S,4S)-4-Hydroxy-3-((3E,7E)-(R)-5-hydroxy-4,8,12-trimethyl-trideca-3,7,11-trienyl)-3,4-dimethyl-2-(3-trityloxy-propyl)-cyclohex-(Z)-ylidene]-propionaldehyde

There total 1 articles about 2-[(2R,3S,4S)-4-Hydroxy-3-((3E,7E)-(R)-5-hydroxy-4,8,12-trimethyl-trideca-3,7,11-trienyl)-3,4-dimethyl-2-(3-trityloxy-propyl)-cyclohex-(Z)-ylidene]-propionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trityl chloride (76-83-5) + (16R)-16-hydroxyiridal → 2-[(2R,3S,4S)-4-Hydroxy-3-((3E,7E)-(R)-5-hydroxy-4,8,12-trimethyl-trideca-3,7,11-trienyl)-3,4-dimethyl-2-(3-trityloxy-propyl)-cyclohex-(Z)-ylidene]-propionaldehyde (219753-50-1)

Guidance literature:

With pyridine; for 24h; Ambient temperature;

DOI:10.1021/np980271b

Reference yield: 12.9%

(R)-methoxytrifluoromethylphenylacetyl chloride (20445-33-4,39637-99-5) + 2-[(2R,3S,4S)-4-Hydroxy-3-((3E,7E)-(R)-5-hydroxy-4,8,12-trimethyl-trideca-3,7,11-trienyl)-3,4-dimethyl-2-(3-trityloxy-propyl)-cyclohex-(Z)-ylidene]-propionaldehyde (219753-50-1) → (S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (E)-(R)-1-{(E)-4-[(1S,2S,6R)-2-hydroxy-1,2-dimethyl-5-[1-methyl-2-oxo-eth-(Z)-ylidene]-6-(3-trityloxy-propyl)-cyclohexyl]-1-methyl-but-1-enyl}-4,8-dimethyl-nona-3,7-dienyl ester

Guidance literature:

With dmap; triethylamine; In dichloromethane; for 15h; Ambient temperature;

DOI:10.1021/np980271b

upstream raw materials:

trityl chloride

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