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Technology Process of Cl4WNC6H4F

Cl4WNC6H4F

Base Information
  • Chemical Name:Cl4WNC6H4F
  • CAS No.:258833-39-5
  • Molecular Formula:C6H4Cl4FNW
  • Molecular Weight:434.765
  • Hs Code.:
Cl<sub>4</sub>WNC<sub>6</sub>H<sub>4</sub>F

Synonyms:

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Chemical Property of Cl4WNC6H4F
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Technology Process of Cl4WNC6H4F

There total 1 articles about Cl4WNC6H4F which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

tungsten(VI) oxychloride

tungsten(VI) oxychloride

para-fluorophenyl isocyanate
1195-45-5

para-fluorophenyl isocyanate

Cl<sub>4</sub>WNC<sub>6</sub>H<sub>4</sub>F
258833-39-5

Cl4WNC6H4F

Guidance literature:
In benzene; byproducts: CO2; addn. of isocyanate to WOCl4 suspension, refluxing 18 h; filtration of hot soln., crystn., washing (pentane), drying (vac.), further crop obtained by concn. of mother liquor, recrystn. (toluene); elem. anal.;
DOI:10.1039/DT9920001663

Reference yield:

Cl<sub>4</sub>WNC<sub>6</sub>H<sub>4</sub>F
258833-39-5

Cl4WNC6H4F

Cl<sub>4</sub>W(C<sub>4</sub>OH<sub>8</sub>)NC<sub>6</sub>H<sub>4</sub>F

Cl4W(C4OH8)NC6H4F

Guidance literature:
With tetrahydrofuran; In tetrahydrofuran; dissolution of complex in THF; evapn. (vac.), washing (pentane), drying (vac.);
DOI:10.1039/DT9920001663
upstream raw materials:

para-fluorophenyl isocyanate

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