((CH₃)2CH)2C₆H₃NHC(C(CH₃)3)NHC₆H₃(CH(CH₃)2)2⁽¹⁺⁾*GeCl₃^(1-)=(((CH₃)2CH)2C₆H₃NHC(C(CH₃)3)NHC₆H₃(CH(CH₃)2)2)GeCl₃

Base Information

• Chemical Name: ((CH₃)2CH)2C₆H₃NHC(C(CH₃)3)NHC₆H₃(CH(CH₃)2)2⁽¹⁺⁾*GeCl₃^(1-)=(((CH₃)2CH)2C₆H₃NHC(C(CH₃)3)NHC₆H₃(CH(CH₃)2)2)GeCl₃
• CAS No.: 1037079-31-4
• Molecular Formula: C₂₉H₄₅N₂*Cl₃Ge
• Molecular Weight: 600.639

Synonyms:

Chemical Property of ((CH₃)2CH)2C₆H₃NHC(C(CH₃)3)NHC₆H₃(CH(CH₃)2)2⁽¹⁺⁾*GeCl₃^(1-)=(((CH₃)2CH)2C₆H₃NHC(C(CH₃)3)NHC₆H₃(CH(CH₃)2)2)GeCl₃

Chemical Property:

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Technology Process of ((CH₃)2CH)2C₆H₃NHC(C(CH₃)3)NHC₆H₃(CH(CH₃)2)2⁽¹⁺⁾*GeCl₃^(1-)=(((CH₃)2CH)2C₆H₃NHC(C(CH₃)3)NHC₆H₃(CH(CH₃)2)2)GeCl₃

There total 2 articles about ((CH₃)2CH)2C₆H₃NHC(C(CH₃)3)NHC₆H₃(CH(CH₃)2)2⁽¹⁺⁾*GeCl₃^(1-)=(((CH₃)2CH)2C₆H₃NHC(C(CH₃)3)NHC₆H₃(CH(CH₃)2)2)GeCl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

germanium(II) chloride dioxane + ((CH3)2CH)2C6H3NHC(C(CH3)3)NHC6H3(CH(CH3)2)2(1+)*Cl(1-)=(((CH3)2CH)2C6H3NHC(C(CH3)3)NHC6H3(CH(CH3)2)2)Cl (1037079-36-9) → ((CH3)2CH)2C6H3NHC(C(CH3)3)NHC6H3(CH(CH3)2)2(1+)*GeCl3(1-)=(((CH3)2CH)2C6H3NHC(C(CH3)3)NHC6H3(CH(CH3)2)2)GeCl3 (1037079-31-4)

Guidance literature:

In tetrahydrofuran; under Ar or N2; soln. of GeCl2*(dioxane) in THF added to soln. of amidinium chloride in THF at -78°C for 5 min; warmed to room temp.; stirred overnight; volatiles removed in vac.; extd. with CH2Cl2; filtered; layered with hexane; crystals isolated; elem. anal.;

DOI:10.1039/b801168k

Reference yield: 18.0%

[(t-Bu)C(N(2,6-(i-Pr)2C6H3))2GeCl] (915151-35-8) + water (7732-18-5) → ((CH3)2CH)2C6H3NHC(C(CH3)3)NHC6H3(CH(CH3)2)2(1+)*GeCl3(1-)=(((CH3)2CH)2C6H3NHC(C(CH3)3)NHC6H3(CH(CH3)2)2)GeCl3 (1037079-31-4)

Guidance literature:

With propylene sulfide; In not given; Ge compd. treated with propylene sulfide; adventitious H2O was present in react. mixt.; mixt. of compds. obtained; only one compd. could be isolated;

DOI:10.1039/b801168k

upstream raw materials:

[(t-Bu)C(N(2,6-(i-Pr)2C₆H₃))2GeCl]

water

((CH₃)2CH)2C₆H₃NHC(C(CH₃)3)NHC₆H₃(CH(CH₃)2)2⁽¹⁺⁾*Cl^(1-)=(((CH₃)2CH)2C₆H₃NHC(C(CH₃)3)NHC₆H₃(CH(CH₃)2)2)Cl

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