6,6-diphenyl-4,4a,5,6,10,10a-hexahydro-2(3H)-anthracenone

Base Information

Chemical Name:6,6-diphenyl-4,4a,5,6,10,10a-hexahydro-2(3H)-anthracenone
CAS No.:123208-72-0
Molecular Formula:C₂₆H₂₄O
Molecular Weight:352.476
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6,6-diphenyl-4,4a,5,6,10,10a-hexahydro-2(3H)-anthracenone

Chemical Property:

Purity/Quality:

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Technology Process of 6,6-diphenyl-4,4a,5,6,10,10a-hexahydro-2(3H)-anthracenone

There total 6 articles about 6,6-diphenyl-4,4a,5,6,10,10a-hexahydro-2(3H)-anthracenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-Hydroxymethyl-3-(3-oxo-butyl)-6,6-diphenyl-3,4,5,6-tetrahydro-4aH-naphthalen-2-one

: 123208-72-0
6,6-diphenyl-4,4a,5,6,10,10a-hexahydro-2(3H)-anthracenone

Guidance literature:: With potassium hydroxide; In 1,4-dioxane; water; for 3h; Yield given; Ambient temperature;
DOI:10.1021/jo00285a028

Reference yield:

: 10346-08-4
3,5-diphenylcyclohex-2-en-1-one

: 123208-72-0
6,6-diphenyl-4,4a,5,6,10,10a-hexahydro-2(3H)-anthracenone

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) NaOMe, / 1.) benzene, 0 deg C, 15 min 2.) 24 h

2: 13.4 g / t-BuOK / 2-methyl-propan-2-ol / 18 h / Ambient temperature

3: KOH / dioxane; H₂O / 5 h / Ambient temperature

4: 1.) MeONa / 1.) benzene, 30 min, 2.) 18 h

5: 1.89 g / t-BuOK / 2-methyl-propan-2-ol / 18 h / Ambient temperature

6: KOH / dioxane; H₂O / 3 h / Ambient temperature

With potassium hydroxide; potassium tert-butylate; sodium methylate; In 1,4-dioxane; water; tert-butyl alcohol;
DOI:10.1021/jo00285a028

Reference yield:

: 123208-73-1
4,4-diphenyl-2-(hydroxymethylene)cyclohex-5-en-1-one

: 123208-72-0
6,6-diphenyl-4,4a,5,6,10,10a-hexahydro-2(3H)-anthracenone

Guidance literature:: Multi-step reaction with 5 steps

1: 13.4 g / t-BuOK / 2-methyl-propan-2-ol / 18 h / Ambient temperature

2: KOH / dioxane; H₂O / 5 h / Ambient temperature

3: 1.) MeONa / 1.) benzene, 30 min, 2.) 18 h

4: 1.89 g / t-BuOK / 2-methyl-propan-2-ol / 18 h / Ambient temperature

5: KOH / dioxane; H₂O / 3 h / Ambient temperature

With potassium hydroxide; potassium tert-butylate; sodium methylate; In 1,4-dioxane; water; tert-butyl alcohol;
DOI:10.1021/jo00285a028