Technology Process of Cyclopentanone, 2-(diphenylphosphinyl)-
There total 10 articles about Cyclopentanone, 2-(diphenylphosphinyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1-(N-morpholino)cyclopent-1-ene; chloro-diphenylphosphine;
With
triethylamine;
In
acetonitrile;
at 0 - 25 ℃;
for 2h;
Inert atmosphere;
With
dimethyl sulfoxide;
In
acetonitrile;
for 2h;
Reflux;
With
hydrogenchloride;
In
water; acetonitrile;
at 0 - 25 ℃;
for 12h;
DOI:10.1002/cbdv.202000217
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / benzene / 24 h
2: hexachloroethane / benzene; petroleum ether
3: 5percent aq. carbonate / CHCl3
With
hexachloroethane; carbonate(2-); triethylamine;
In
chloroform; Petroleum ether; benzene;
- Guidance literature:
-
With
oxygen;
In
tetrahydrofuran;
for 0.5h;
Ambient temperature;
DOI:10.1021/jo00291a018
