1,7-bis(tosyl) trisulfur tetranitride

Base Information

• Chemical Name: 1,7-bis(tosyl) trisulfur tetranitride
• CAS No.: 120263-51-6
• Molecular Formula: C₁₄H₁₄N₄O₄S₅
• Molecular Weight: 462.62
• Mol file: 120263-51-6.mol

Synonyms:

Chemical Property of 1,7-bis(tosyl) trisulfur tetranitride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,7-bis(tosyl) trisulfur tetranitride

There total 3 articles about 1,7-bis(tosyl) trisulfur tetranitride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

N'-tosyl-N-(trimethylsilyl)sulfur diimide (120263-52-7) → 1,7-bis(tosyl) trisulfur tetranitride (120263-51-6)

Guidance literature:

With sulfur dichloride; In diethyl ether; for 72h; Ambient temperature;

Reference yield: 36.0%

N,N'-bis(trimethylsilyl)sulfurdiimide (503027-47-2,503027-48-3,155139-78-9,18156-25-7) + (toluene-4-sulfonyl)-imidosulfurous acid dichloride (33840-97-0) → 1,7-bis(tosyl) trisulfur tetranitride (120263-51-6)

Guidance literature:

In diethyl ether; for 72h; Ambient temperature;

Reference yield:

(toluene-4-sulfonyl)-imidosulfurous acid dichloride (33840-97-0) → 1,7-bis(tosyl) trisulfur tetranitride (120263-51-6)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / 24 h / Ambient temperature

2: 43 percent / SCl₂ / diethyl ether / 72 h / Ambient temperature

With sulfur dichloride; In diethyl ether; dichloromethane;

upstream raw materials:

N,N'-bis(trimethylsilyl)sulfurdiimide

(toluene-4-sulfonyl)-imidosulfurous acid dichloride

N'-tosyl-N-(trimethylsilyl)sulfur diimide

Downstream raw materials:

S,S-dimethyl-N-p-tolylsulfonylsulfimine

1-(3,6-dihydro-4,5-dimethyl-2-tosyl-2H-1,2-thiazin-1-ylidene)-5-tosyl disulfur trinitride

Refernces