naphthalenechromium dicarbonyl triphenylphosphite

Base Information

Chemical Name:naphthalenechromium dicarbonyl triphenylphosphite
CAS No.:73656-20-9
Molecular Formula:C₃₀H₂₃CrO₅P
Molecular Weight:546.479
Hs Code.:

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Chemical Property of naphthalenechromium dicarbonyl triphenylphosphite

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Technology Process of naphthalenechromium dicarbonyl triphenylphosphite

There total 1 articles about naphthalenechromium dicarbonyl triphenylphosphite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101-02-0
triphenyl phosphite

: 12110-37-1
tricarbonyl(naphthalene)chromium⁽⁰⁾

: 73656-20-9
naphthalenechromium dicarbonyl triphenylphosphite

Guidance literature:: With C₄H₈O; In tetrahydrofuran; Irradiation (UV/VIS); (N2); soln. of Cr complex was UV irradiated until Cr-THF complex had formed, monitored by IR, then equimolar amt. of ligand was added and soln.was allowed to stand for 30 min at room temp.; soln. was evapd. under vac., residue dissolved in benzene/PE (1/1) and chromd. (silicagel, benzene/PE, first 1/1, increasing benzene content), last band yielded product; recrystn. from cyclohexane/PE;
DOI:10.1016/S0022-328X(00)94367-5