phenyl-3 exo bicyclo<2.2.1>heptane carbolactone 2-6

Base Information

• Chemical Name: phenyl-3 exo bicyclo<2.2.1>heptane carbolactone 2-6
• CAS No.: 81509-28-6
• Molecular Formula: C₁₄H₁₄O₂
• Molecular Weight: 214.264

Synonyms:

Chemical Property of phenyl-3 exo bicyclo<2.2.1>heptane carbolactone 2-6

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of phenyl-3 exo bicyclo<2.2.1>heptane carbolactone 2-6

There total 9 articles about phenyl-3 exo bicyclo<2.2.1>heptane carbolactone 2-6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ phenyl-3 exo bicyclo<2.2.1>heptane carbolactone 2-6 (81509-28-6,81570-47-0)

Guidance literature:

With pyridine; ethanol; nickel; Hydrogenation;

DOI:10.1021/ja01623a058

Reference yield:

endo-5-carboxy-exo-6-phenylbicyclo<2.2.1>hept-2-ene (6319-19-3,58800-36-5,59286-05-4,59286-09-8,59286-12-3,67711-15-3,67711-16-4,130793-98-5) → phenyl-3 exo bicyclo<2.2.1>heptane carbolactone 2-6 (81509-28-6,81570-47-0)

Guidance literature:

With sodium tetrahydroborate; Yield given. Multistep reaction; 1.) oxymercuration;

DOI:10.1016/S0040-4020(01)98883-0

Reference yield:

3-endo-phenylnorborn-5-ene-2-endo-ylcarboxylic acid (6319-19-3,58800-36-5,59286-05-4,59286-09-8,59286-12-3,67711-15-3,67711-16-4,130793-98-5) → phenyl-3 endo bicyclo<2.2.1>heptane carbolactone 2-6 (81509-28-6,81570-47-0)

Guidance literature:

With sodium tetrahydroborate; Yield given. Multistep reaction; 1.) oxymercuration;

DOI:10.1016/S0040-4020(01)98883-0

upstream raw materials:

endo-5-carboxy-exo-6-phenylbicyclo<2.2.1>hept-2-ene

(E)-3-phenylacrylic acid

cyclopenta-1,3-diene

endo-6-hydroxy-5-iodo-3-phenylbicyclo[2.2.1]heptane-2-carboxylic acid lactone

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